Analysis of the New Metals


Book Description

Analysis of the New Metals: Titanium, Zirconium, Hafnium, Niobium, Tantalum, Tungsten and their Alloys focuses on methods for the analysis of titanium, zirconium, hafnium, niobium, tantalum, tungsten, and their alloys. Emphasis is on the procedures used in Imperial Metal Industries (Kynoch) Limited's laboratories for the analysis of these metals. These procedures include the oxide-resin procedure, solution procedure, and the point-to-plane spectrographic procedure. Comprised of six chapters, this book begins with an overview of special procedures for obtaining representative samples, including the use of titanium or zirconium sponge (Kroll process) as well as titanium granules (ICI sodium process). Subsequent chapters discuss the identification of titanium and its alloys such as aluminum, boron, calcium, carbon, and copper by means of the point-to-plane spectrographic procedure, a Fuess metal spectroscope, and chemical spot-tests; spectroscopic analysis of zirconium, zirconium alloys, and ionide-refined hafnium; and spectroscopic analysis of niobium, tantalum, tungsten, and their alloys. This monograph will be useful for undergraduate students, educators, practitioners, and researchers in metallurgy.




Trace Elemental Analysis of Metals


Book Description

This work details minor, trace and ultratrace methods; addresses the essential stages that precede measurement; and highlights the measurement systems most likey to be used by the pragmatic analyst. It features key material on inclusion and phase isolation. The book is designed to provide useful maps and signposts for metals analysts who must verify that stringent trace level compositional specifications have been met.




Metal Failures


Book Description

comprehensive coverage of both the "how" and "why" of metal failures Metal Failures gives engineers the intellectual tools and practical understanding needed to analyze failures from a structural point of view. Its proven methods of examination and analysis enable investigators to: * Reach correct, fact-based conclusions on the causes of metal failures * Present and defend these conclusions before highly critical bodies * Suggest design improvements that may prevent future failures Analytical methods presented include stress analysis, fracture mechanics, fatigue analysis, corrosion science, and nondestructive testing. Numerous case studies illustrate the application of basic principles of metallurgy and failure analysis to a wide variety of real-world situations. Readers learn how to investigate and analyze failures that involve: * Alloys and coatings * Brittle and ductile fractures * Thermal and residual stresses * Creep and fatigue * Corrosion, hydrogen embrittlement, and stress-corrosion cracking This useful professional reference is also an excellent learning tool for senior-level students in mechanical, materials, and civil engineering.













Analysis of Ancient Metals


Book Description

Analysis of Ancient Metals provides a guide to the identification and analysis of ancient metals and alloys. The title details the various analytical methods and procedures in dealing with different metals and alloys. The text first discusses the heterogeneity of ancient metals and the sampling problem, and then proceeds to covering preliminary observations and measurements, qualitative tests, and choice of quantitative method. The next series of chapters details the methods and procedures in the analysis of gold, silver, copper, iron, and steel, as well as various nonferrous metals. The last chapter discusses the concerns in reporting the findings. The book will be of great interest to materials engineers and metallurgists. Archeologists and museologists will also greatly benefit from the text.




Systematic Materials Analysis


Book Description

Systematic Materials Analysis, Volume III presents brief discussions on a broad range of instrumental methods and approaches that will yield the desired information about a given material. The book discusses the selection of analytical methods on the bases of specimen limitations and information desired. The chapters on specific instruments briefly outline the theories of operation and describe the capability of the methods for qualitative and quantitative measurements of chemical composition, structure, and texture (as applicable). The commercial instruments and techniques discussed include arc, spark, laser, plasmas, flame photometry, gas analysis techniques, combustion methods, gas chromatography, and ion-scattering spectrometry. The Mossbauer spectrometry; optical microscopy; x-ray diffraction; x-ray fluorescence; and absorption spectrometry are also encompassed. Materials analyst, materials scientist, chemists, and engineers will find the book invaluable.







Systematic Materials Analysis Part 1


Book Description

Systematic Materials Analysis focuses on the broad range of instrumental methods that brings new approaches to materials analysts to yield the desired information about a given material. This book explores the specific instruments that briefly outline the theories of operation. Organized into ten chapters, this volume starts with an overview of the analytical methods on the bases of specimen limitations and information desired, and then examines the use of flow charts encompassing the various instruments. This text then discusses the use of the charts, which present a complete listing of analytical instrumentation arranged so as to enable the selection of the best method for a given analytical task. Other chapters outline the theories of operation and describe the capability of the methods for quantitative and qualitative measurements of chemical composition, texture, and structure as applicable. This book is a valuable resource for materials analysts, engineers, biological scientists, laboratory administrators, and researchers.