Analytical Methods and Instruments for Micro- and Nanomaterials


Book Description

This book describes analytical instruments widely used to characterize the nanostructured materials. It provides information about how to assess material quality, defects, the state of surfaces and interfaces, element distributions, strain, lattice distortion, and electro-optical properties of materials and devices. The information provided by this book can be used as a back-up for material processing, material design and debugging of device performance. The basic principles and methodology of each analysis technique is described in separate chapters, adding historic perspectives and recent developments. The data analysis, from simple to advanced level, is introduced by numerous examples, mostly taken from the authors' fields of research; semiconductor materials, metals and oxides. The book serves as a valuable guide for scientists and students working in materials science, physics, and engineering, who wish to become acquainted with the most important analytical techniques for nanomaterials.




Analytical Methods and Instruments for Micro- and Nanomaterials


Book Description

This book describes analytical instruments widely used to characterize the nanostructured materials. It provides information about how to assess material quality, defects, the state of surfaces and interfaces, element distributions, strain, lattice distortion, and electro-optical properties of materials and devices. The information provided by this book can be used as a back-up for material processing, material design and debugging of device performance. The basic principles and methodology of each analysis technique is described in separate chapters, adding historic perspectives and recent developments. The data analysis, from simple to advanced level, is introduced by numerous examples, mostly taken from the authors' fields of research; semiconductor materials, metals and oxides. The book serves as a valuable guide for scientists and students working in materials science, physics, and engineering, who wish to become acquainted with the most important analytical techniques for nanomaterials.




Analytical Sample Preparation With Nano- and Other High-Performance Materials


Book Description

Analytical Sample Preparation With Nano- and Other High-Performance Materials covers advanced sample treatment techniques and the new materials that can be used to boost their performance. The evolution of sample treatment over the last two decades has resulted in the development of new techniques and application of new materials. This is a must-have resource for those studying advanced analytical techniques and the role of high-performance materials in analytical chemistry. The book explains the underlying principles needed to properly understand sample preparation, and also examines the latest materials - including nanomaterials - that result in greater sensitivity and specificity. The book begins with a section devoted to all the various sample preparation techniques and then continues with sections on high-performance sorbents and high-performance solvents. - Combines basic, fundamental principles and advanced concepts and applications for a comprehensive treatment of sample preparation with new materials - Defines nano- and other high-performance materials in this context, including carbon nanoparticles, inorganic nanoparticles, ionic liquids, supramolecular solvents, and more - Includes discussion of all the latest advancements and new findings in both techniques and materials used for proper sample preparation




Micro- and Nanotechnology Enabled Applications for Portable Miniaturized Analytical Systems


Book Description

Micro- and Nanotechnology Enabled Applications for Portable Miniaturized Analytical Systems outlines the basic principles of miniaturized analytical devices, such as spectrometric, separation, imaging and electrochemical miniaturized instruments. Concepts such as smartphone-enabled miniaturized detection systems and micro/nanomachines are also reviewed. Subsequent chapters explore the emerging application of these mobile devices for miniaturized analysis in various fields, including medicine and biomedicine, environmental chemistry, food chemistry, and forensic chemistry. This is an important reference source for materials scientists and engineers wanting to understand how miniaturization techniques are being used to create a range of efficient, sustainable electronic and optical devices. Miniaturization describes the concept of manufacturing increasingly smaller mechanical, optical, and electronic products and devices. These smaller instruments can be used to produce micro- and nanoscale components required for analytical procedures. A variety of micro/nanoscale materials have been synthesized and used in analytical procedures, such as sensing materials, sorbents, adsorbents, catalysts, and reactors. The miniaturization of analytical instruments can be applied to the different steps of analytical procedures, such as sample preparation, analytical separation, and detection, reducing the total cost of manufacturing the instruments and the needed reagents and organic solvents. Outlines how miniaturization techniques can be used to create new optical and electronic micro- and nanodevices Explores major application areas, including biomedicine, environmental science and security Assesses the major challenges of using miniaturization techniques




Micro- and Nanotechnology Enabled Applications for Portable Miniaturized Analytical Systems


Book Description

Micro- and Nanotechnology Enabled Applications for Portable Miniaturized Analytical Systems outlines the basic principles of miniaturized analytical devices, such as spectrometric, separation, imaging and electrochemical miniaturized instruments. Concepts such as smartphone-enabled miniaturized detection systems and micro/nanomachines are also reviewed. Subsequent chapters explore the emerging application of these mobile devices for miniaturized analysis in various fields, including medicine and biomedicine, environmental chemistry, food chemistry, and forensic chemistry. This is an important reference source for materials scientists and engineers wanting to understand how miniaturization techniques are being used to create a range of efficient, sustainable electronic and optical devices. Miniaturization describes the concept of manufacturing increasingly smaller mechanical, optical, and electronic products and devices. These smaller instruments can be used to produce micro- and nanoscale components required for analytical procedures. A variety of micro/nanoscale materials have been synthesized and used in analytical procedures, such as sensing materials, sorbents, adsorbents, catalysts, and reactors. The miniaturization of analytical instruments can be applied to the different steps of analytical procedures, such as sample preparation, analytical separation, and detection, reducing the total cost of manufacturing the instruments and the needed reagents and organic solvents. - Outlines how miniaturization techniques can be used to create new optical and electronic micro- and nanodevices - Explores major application areas, including biomedicine, environmental science and security - Assesses the major challenges of using miniaturization techniques




Analytical Nanochemistry


Book Description

Analytical Nanochemistry provides readers with a comprehensive review of the application of nanomaterial in analytical chemistry. It explains the fundamental concepts involved in utilizing nanomaterials including their classification, synthesis, functionalization, characterization methods, separation, and isolation techniques, as well as toxicity. It also covers fundamental information on different aspects of analytical procedures and method development. Furthermore, it emphasizes micro- and nano-enabled analytical devices and instruments as well as nanotools for nanoanalysis. The book opens with a section on fundamentals (Section 1), then continues with a section on the role of nanomaterials in analytical procedures (Section 2), including sample preparation, separation, and detection. The third section (Section 3) includes chapters on micro- and nano-enabled devices, as most miniaturized microsystems include nanofeatures. The book concludes with a fourth section (Section 4) on future perspectives, covering nanoanalysis, bioanalysis, toxic risks, and limitations of both technology and commercialization. This book serves as a valuable resource for students, instructors, and researchers in analytical chemistry, nanomaterials, and nanotechnology investigating the use of nanotechnology in their analytical procedures. - Covers the synthesis methods, functionalization process, and characterization methods of nanomaterials - Uses numerous visual elements to illustrate key points, including flowcharts, process diagrams, photographs, and visual schemes - Presents fundamental concepts and updated hot topics such as miniaturization in analytical chemistry, nanotools for nano-analysis, micro total analysis systems, and lab-on-a-chip







High-Entropy Alloys


Book Description

High-Entropy Alloys: Design, Manufacturing, and Emerging Applications presents cutting-edge advances in the field of these materials, covering their mechanics, methods of manufacturing, and applications, all while emphasizing the link between their structure/microstructure and functional properties. The book starts with a section on the fundamentals of high-entropy alloys (HEAs), with chapters discussing their thermodynamics, subgroups (transition metal; refractory; ceramics; metallic glasses and more), physical metallurgy, and microstructural characterization. The next section features chapters which look at manufacturing processes of HEAs, such as liquid metallurgy synthesis, in-situ synthesis, additive manufacturing, machine learning, friction stir welding, and fabrication of coatings for HEAs. The final section of the book covers applications of these materials, including their use as irradiation-resistant structural materials, catalyst materials, electrode materials, HEAs for solid hydrogen storage, and more. The book is a key resource for academic researchers, grad students, and industry professionals working with HEAs across a range of disciplines and applications including aerospace, functional materials, catalyst materials, gas storage, sensing, super-conducting materials, biomedical, civil engineering, energy storage, and energy materials. - Covers the mechanics, manufacturing, and applications of functionally-oriented high-entropy alloys (HEAs) - Discusses the metallurgical composition of HEAs, their microstructural characterization, thermal stability, and how to manufacture them via powder metallurgy, additive manufacturing, and friction stir welding - Reviews applications of HEAs such as for irradiation-resistant structural materials, in biomedical settings, as catalyst materials, for solid hydrogen storage, and more




Nanobotany


Book Description

This work synthesizes research and practical work, including various techniques and applications of botany and nanoparticles, including enzymology, pharmaceuticals, phenolics, antioxidants, metal particles, synthesis of nanoparticles by plants and microbes, and more. The text discusses the latest research as well as key sources of information condensed from other scholars across the globe, providing a comprehensive resource for scholars working in nanobotany, as well as chemists and researchers in the pharmaceutical industry.




Miniaturized Analytical Devices


Book Description

Miniaturized Analytical Devices An in-depth overview of integrating functionalized nanomaterials with mass spectrometry, spectroscopy, electrophoresis, and other important analytical techniques Miniaturized Analytical Devices: Materials and Technology is an up-to-date resource exploring the analytical applications of miniaturized technology in areas such as clinical microbiology, pharmaceuticals, agriculture, and environmental analysis. The book covers the integration of functional nanomaterials in mass spectrometry, microscopy, electrophoresis, and more—providing the state-of-the-art information required for successfully implementing a range of chemical analysis techniques on microchips. Featuring contributions from a panel of international experts in the field, the book begins with an introduction to selected miniaturized devices, nanomaterials, and analytical methods. Subsequent sections describe functionalized nanomaterials (FNMs) for miniaturized devices and discuss techniques such as miniaturized mass spectrometry for bioassays and miniaturized microscopy for cell imaging. The book concludes by exploring a variety of applications of miniaturized devices in areas including metal analysis, bioimaging, DNA separation and analysis, molecular biology, and more. This timely volume: Surveys the current state of the field and provides a starting point for developing faster, more reliable, and more selective analytical devices Focuses on the practical applications of miniaturized analytical devices in materials science, clinical microbiology, the pharmaceutical industry, and environmental analysis Covers a wide range of materials and analytical techniques such as microvolume UV-VIS spectroscopy, microchip and capillary electrophoresis, and matrix assisted laser desorption ionization-mass spectrometry (MALDI-MS) analysis Discusses the role of miniaturized analytical devices in securing a green and sustainable future Miniaturized Analytical Devices: Materials and Technology is essential reading for analytical chemists, analytical laboratories, materials scientists, biologists, life scientists, and advanced students in related fields.