Author : Stefan Mathias Sarge
Publisher : John Wiley & Sons
Page : 346 pages
File Size : 29,43 MB
Release : 2014-02-25
Category : Science
ISBN : 3527649387
Clearly divided into three parts, this practical book begins by dealing with all fundamental aspects of calorimetry. The second part looks at the equipment used and new developments. The third and final section provides measurement guidelines in order to obtain the best results. The result is optimized knowledge for users of this technique, supplemented with practical tips and tricks.
Author : G.W.H. Höhne
Publisher : Springer Science & Business Media
Page : 233 pages
File Size : 26,93 MB
Release : 2013-06-29
Category : Science
ISBN : 366203302X
Differential Scanning Calorimetry (DSC) is a well established measuring method which is used on a large scale in different areas of research, development, and quality inspection and testing. Over a large temperature range, thermal effects can be quickly identified and the relevant temperature and the characteristic caloric values determined using substance quantities in the mg range. Measurement values obtained by DSC allow heat capacity, heat of transition, kinetic data, purity and glass transition to be determined. DSC curves serve to identify substances, to set up phase diagrams and to determine degrees of crystallinity. This book provides, for the first time, an overall description of the most impor tant applications of Differential Scanning Calorimetry. Prerequisites for reliable measurement results, optimum evaluation of the measurement curves and esti mation of the uncertainties of measurement are, however, the knowledge of the theoretical bases of DSC, a precise calibration of the calorimeter and the correct analysis of the measurement curve. The largest part of this book deals with these basic aspects: The theory of DSC is discussed for both heat flux and power compensated instruments; temperature calibration and caloric calibration are described on the basis of thermodynamic principles. Desmearing of the measurement curve in different ways is presented as a method for evaluating the curves of fast transitions.
Author : Richard B. Kemp
Publisher : Elsevier
Page : 1061 pages
File Size : 12,26 MB
Release : 1999-12-13
Category : Science
ISBN : 0080535690
The applications and interest in thermal analysis and calorimetry have grown enormously during the last half of the 20th century. These techniques have become indispensable in the study of processes such as catalysis, hazards evaluation etc., and in measuring important physical properties quickly, conveniently and with markedly improved accuracy. Consequently, thermal analysis and calorimetry have grown in stature and more scientists and engineers have become at least part-time, practitioners. People new to the field therefore need a source of information describing the basic principles and current state of the art. The last volume of this 4 volume handbook, devoted to many aspects of biological thermal analysis and calorimetry, completes a comprehensive review of this important area. All chapters have been prepared by recognized experts in their respective fields. The approach taken is "how and what to do and when to do it". The complete work is a valuable addition to the already existing literature.
Author : Michael E. Brown
Publisher : Elsevier
Page : 725 pages
File Size : 44,75 MB
Release : 1998-09-07
Category : Science
ISBN : 0080539599
Handbook of Thermal Analysis and Calorimetry, Volume 1: Principles and Practice describes the basic background information common to thermal analysis and calorimetry in general. Thermodynamic and kinetic principles are discussed along with the instrumentation and methodology associated with thermoanalytical and calorimetric techniques. The purpose is to collect the discussion of these general principles and minimize redundancies in the subsequent volumes that are concerned with the applications of these principles and methods. More unique methods, which pertain to specific processes or materials, are covered in later volumes.
Author : R. Wigmans
Publisher : Oxford University Press
Page : 732 pages
File Size : 34,43 MB
Release : 2000
Category : Calorimetry
ISBN : 9780198502968
Particle physics is the science that pursues the age-old quest for the innermost structure of matter and the fundamental interactions between its constituents. Modern experiments in this field rely increasingly on calorimetry, a detection techniques in which the particles of interest are absorbed in the detector. Calorimeters are very intricate instruments, their performance characteristics depend in subtle, sometimes counter-intuitive ways on design details. This book, written by one of the world's foremost experts, is the first comprehensive text on this topic. It provides a fundamental and systematic introduction, in which many intriguing calorimeter features are explained. It also describes the state of the art, both for what concerns the fundamental understanding of calorimetric particle detection and the actual detectors that have been or are being built and operated in experiments. In the last chapter, some landmark scientific discoveries in which calorimetry has played an important role are discussed. This book summarizes and puts into perspective work described in some 600 scientific papers, listed in the bibliography.
Author : Paul Flowers
Publisher :
Page : 0 pages
File Size : 44,7 MB
Release : 2019-02-14
Category : Chemistry
ISBN : 9781947172623
Chemistry 2e is designed to meet the scope and sequence requirements of the two-semester general chemistry course. The textbook provides an important opportunity for students to learn the core concepts of chemistry and understand how those concepts apply to their lives and the world around them. The book also includes a number of innovative features, including interactive exercises and real-world applications, designed to enhance student learning. The second edition has been revised to incorporate clearer, more current, and more dynamic explanations, while maintaining the same organization as the first edition. Substantial improvements have been made in the figures, illustrations, and example exercises that support the text narrative. Changes made in Chemistry 2e are described in the preface to help instructors transition to the second edition.
Author : Amal Ali Elkordy
Publisher : BoD – Books on Demand
Page : 488 pages
File Size : 31,57 MB
Release : 2013-01-23
Category : Science
ISBN : 9535109472
Calorimetry, as a technique for thermal analysis, has a wide range of applications which are not only limited to studying the thermal characterisation (e.g. melting temperature, denaturation temperature and enthalpy change) of small and large drug molecules, but are also extended to characterisation of fuel, metals and oils. Differential Scanning Calorimetry is used to study the thermal behaviours of drug molecules and excipients by measuring the differential heat flow needed to maintain the temperature difference between the sample and reference cells equal to zero upon heating at a controlled programmed rate. Microcalorimetry is used to study the thermal transition and folding of biological macromolecules in dilute solutions. Microcalorimetry is applied in formulation and stabilisation of therapeutic proteins. This book presents research from all over the world on the applications of calorimetry on both solid and liquid states of materials.
Author :
Publisher : Elsevier
Page : 862 pages
File Size : 21,78 MB
Release : 2018-03-12
Category : Technology & Engineering
ISBN : 0444640630
Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. - Features 19 all-new chapters to bring readers up to date on the current status of the field - Provides a broad overview of recent progress in the most popular techniques and applications - Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry - Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics - Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications
Author : Michio Sorai
Publisher : John Wiley & Sons
Page : 570 pages
File Size : 13,26 MB
Release : 2004-09-03
Category : Science
ISBN :
Publisher Description
Author : Stig Sunner
Publisher : Elsevier
Page : 455 pages
File Size : 20,73 MB
Release : 2016-06-03
Category : Science
ISBN : 1483280896
Experimental Chemical Thermodynamics, Volume 1: Combustion Calorimetry covers the advances in calorimetric study of combustion, with particular emphasis on the accuracy of the method. This book is composed of 18 chapters, and begins with a presentation of the units and physical constants with the basic units of measurements. The succeeding chapters deal with basic principles of combustion calorimetry, emphasizing the underlying basic principles of measurement. These topics are followed by discussions on calibration of combustion calorimeters, test and auxiliary substances in combustion calorimetry, strategies in the calculation of standard-state energies of combustion from the experimentally determined quantities, and assignment of uncertainties. The final chapter considers the history of combustion calorimetry. This book will prove useful to combustion chemists and engineers, as well as researchers in the allied fields.
