Design and Control of Distillation Systems for Separating Azeotropes


Book Description

Hands-on guidance for the design, control, and operation of azeotropic distillation systems Following this book's step-by-step guidance, readers learn to master tested and proven methods to overcome a major problem in chemical processing: the distillation and separation of azeotropes. Practical in focus, the book fully details the design, control, and operation of azeotropic distillation systems, using rigorous steady-state and dynamic simulation tools. Design and Control of Distillation Systems for Separating Azeotropes is divided into five parts: Fundamentals and tools Separations without adding other components Separations using light entrainer (heterogeneous azeotropic distillation) Separations using heavy entrainer (extractive distillation) Other ways for separating azeotropes The distillation methods presented cover a variety of important industrial chemical systems, including the processing of biofuels. For most of these chemical systems, the authors explain how to achieve economically optimum steady-state designs. Moreover, readers learn how to implement practical control structures that provide effective load rejection to manage disturbances in throughput and feed composition. Trade-offs between steady-state energy savings and dynamic controllability are discussed, helping readers design and implement the distillation system that best meets their particular needs. In addition, economic and dynamic comparisons between alternative methods are presented, including an example of azeotropic distillation versus extractive distillation for the isopropanol/water system. With its focus on practical solutions, Design and Control of Distillation Systems for Separating Azeotropes is ideal for engineers facing a broad range of azeotropic separation problems. Moreover, this book is recommended as a supplemental text for undergraduate and graduate engineering courses in design, control, mass transfer, and bio-processing.




Conceptual Design of Distillation Systems with CD-ROM


Book Description

This book is a pioneering effort by two of the world's top researchers. The authors have fashioned a text which develops models, the basis for software tools for conceptual design. The book clearly addresses both analysis and design with sharp attention to supplying mathematical correctness and providing physical insight. A software supplement accompanies the text in a student version.







Distillation


Book Description

Distillation: Fundamentals and Principles — winner of the 2015 PROSE Award in Chemistry & Physics — is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on the conceptual design of distillation. - Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers - Practical information on the newest development written by recognized experts - Coverage of a huge range of laboratory and industrial distillation approaches - Extensive references for each chapter facilitates further study




European Symposium on Computer Aided Process Engineering - 11


Book Description

This book contains papers presented at the 11th Symposium of Computer Aided Process Engineering (ESCAPE-11), held in Kolding, Denmark, from May 27-30, 2001. The objective of ESCAPE-11 is to highlight the use of computers and information technology tools, that is, the traditional CAPE topics as well as the new CAPE topics of current and future interests.The main theme for ESCAPE-11 is process and tools integration with emphasis on hybrid processing, cleaner and efficient technologies (process integration), computer aided systems for modelling, design, synthesis, control (tools integration) and industrial case studies (application of integrated strategies). The papers are arranged in terms of the following themes: computer aided control/operations, computer aided manufacturing, process and tools integration, and new frontiers in CAPE. A total of 188 papers, consisting of 5 keynote and 183 contributed papers are included in this book.




Chemical Engineering Design


Book Description

Chemical Engineering Design, Second Edition, deals with the application of chemical engineering principles to the design of chemical processes and equipment. Revised throughout, this edition has been specifically developed for the U.S. market. It provides the latest US codes and standards, including API, ASME and ISA design codes and ANSI standards. It contains new discussions of conceptual plant design, flowsheet development, and revamp design; extended coverage of capital cost estimation, process costing, and economics; and new chapters on equipment selection, reactor design, and solids handling processes. A rigorous pedagogy assists learning, with detailed worked examples, end of chapter exercises, plus supporting data, and Excel spreadsheet calculations, plus over 150 Patent References for downloading from the companion website. Extensive instructor resources, including 1170 lecture slides and a fully worked solutions manual are available to adopting instructors. This text is designed for chemical and biochemical engineering students (senior undergraduate year, plus appropriate for capstone design courses where taken, plus graduates) and lecturers/tutors, and professionals in industry (chemical process, biochemical, pharmaceutical, petrochemical sectors). New to this edition: - Revised organization into Part I: Process Design, and Part II: Plant Design. The broad themes of Part I are flowsheet development, economic analysis, safety and environmental impact and optimization. Part II contains chapters on equipment design and selection that can be used as supplements to a lecture course or as essential references for students or practicing engineers working on design projects. - New discussion of conceptual plant design, flowsheet development and revamp design - Significantly increased coverage of capital cost estimation, process costing and economics - New chapters on equipment selection, reactor design and solids handling processes - New sections on fermentation, adsorption, membrane separations, ion exchange and chromatography - Increased coverage of batch processing, food, pharmaceutical and biological processes - All equipment chapters in Part II revised and updated with current information - Updated throughout for latest US codes and standards, including API, ASME and ISA design codes and ANSI standards - Additional worked examples and homework problems - The most complete and up to date coverage of equipment selection - 108 realistic commercial design projects from diverse industries - A rigorous pedagogy assists learning, with detailed worked examples, end of chapter exercises, plus supporting data and Excel spreadsheet calculations plus over 150 Patent References, for downloading from the companion website - Extensive instructor resources: 1170 lecture slides plus fully worked solutions manual available to adopting instructors




Purification of Laboratory Chemicals


Book Description

Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.* Complete update of this valuable, well-known reference* Provides purification procedures of commercially available chemicals and biochemicals* Includes an extremely useful compilation of ionisation constants




Guide to Capital Cost Estimating


Book Description

Known as the Blue Book this fourth edition continues with the endorsement from the Association of Cost Engineers. The guide is designed to be an aid for student engineers in the design activities undertaken during their course and help young engineers in industry to compile their own set of cost data. With much of the material in the third edition retained, the major changes are: new cost data; up-dated cost index information (which has been donated by industrialists); and short-cut estimating techniques up-dated.




Distillation Theory and its Application to Optimal Design of Separation Units


Book Description

Originally published in 2004, Distillation Theory and Its Application to Optimal Design of Separation Units presents a clear, multidimensional geometric representation of distillation theory that is valid for all distillation column types, splits, and mixtures. This representation answers such fundamental questions as: what are the feasible separation products for a given mixture? What minimum power is required to separate a given mixture? What minimum number of trays is necessary to separate a given mixture at a fixed power input? This book is intended for students and specialists in the design and operation of separation units in the chemical, pharmaceutical, food, wood, petrochemical, oil-refining, and natural gas industries and for software designers.




Chemical Process Design


Book Description

This practical how-to-do book deals with the design of sustainable chemical processes by means of systematic methods aided by computer simulation. Ample case studies illustrate generic creative issues, as well as the efficient use of simulation techniques, with each one standing for an important issue taken from practice. The didactic approach guides readers from basic knowledge to mastering complex flow-sheets, starting with chemistry and thermodynamics, via process synthesis, efficient use of energy and waste minimization, right up to plant-wide control and process dynamics. The simulation results are compared with flow-sheets and performance indices of actual industrial licensed processes, while the complete input data for all the case studies is also provided, allowing readers to reproduce the results with their own simulators. For everyone interested in the design of innovative chemical processes.