Modern Polarographic Methods in Analytical Chemistry


Book Description

This book provides up-to-date discussion of modern polarographic methods, with examples and experimental details. It is designed for the practicing analyst and a factor in bringing the reincarnated area of analytical chemistry into a new and healthy maturity.




Modern Methods of Pharmaceutical Analysis, Second Edition


Book Description

This book reviews several of the newer methods that find wide application in pharmaceutical analysis, as well as several older methods of unique importance. The principle of each technique is discussed with emphasis on factors that directly affect its proper application to analytical problems .




Organic Polarographic Analysis


Book Description

Organic Polarographic Analysis deals with the applications of polarography in the analysis of organic compounds. The principles, techniques, and apparatus of organic polarography are discussed, and some selected examples of the applications of organic polarography in various fields of applied chemistry are presented. The direct methods in which the sample is simply dissolved in a suitable supporting electrolyte are also considered. This book consists of 11 chapters and opens with an overview of the basic principles of the polarographic method of analysis, as well as the different types of polarographic limiting currents and of electrode processes. The reader is then introduced to the instruments used in polarography, including the polarograph, dropping and reference electrodes, and electrolysis vessels. Experimental techniques in organic polarography are also described, along with some of its practical applications in fields such as pharmacy, medicine, and biochemistry. Subsequent chapters explore polarographic methods used in the analysis of organic substances, including direct and indirect methods of analysis; separation techniques; and the use of polarography in organic synthesis and isolation of natural products. This monograph is written primarily for organic and analytical chemists.




Principles of Polarography


Book Description

Principles of Polarography is a revised and extended version of an original Czech edition that appeared in 1962 at the Publishing House of the Czechoslovak Academy of Sciences in Prague. Based on a one-term course of lectures for third-year students of chemistry at the Charles University it brings the fundamental results of more than forty years' research in the field of polarography. The book contains 22 chapters and opens with a discussion of the principles of polarography. This is followed by separate chapters on polarizable electrodes used in polarography; charging current; influence of the resistance of the electrolyte on polarographic curves; migration and diffusion-controlled currents; and equation of a reversible polarographic wave. Subsequent chapters deal with reversible processes controlled by diffusion of complex ions; reversible reduction of organic substances; deposition of mercury ions; irreversible electrode processes; applications of limiting currents; polarographic curves for the formation of semiquinones and dimers; and catalytic hydrogen currents.




POLAROGRAPHY AND OTHER VOLTAMMETRIC METHODS (SET PRICE OF 34 BOOKS)


Book Description

The book introduces a wide range of voltammetric techniques, covering basic theory, practical aspects, and the scope of each technique. The book shows how to select suitable methods for particular applications and prepares the reader for further study of individual techniques. Introduces the discipline's terminology, makes clear how to choose operating parameters, and how to research the literature. It contains self-assessment questions and responses, units of measurement, a glossary, and abbreviations used in electrochemistry. · Classical dc Polarography· Electrode Processes· Pulse Polarographic Techniques· Stripping Voltammetry· Polarography/Voltammetry and the Analyst· Self Assessment Questions and Responses· Units of Measurement· Glossary and Abbreviations Used in Electrochemistry




Instrumentation Reference Book


Book Description

The discipline of instrumentation has grown appreciably in recent years because of advances in sensor technology and in the interconnectivity of sensors, computers and control systems. This 4e of the Instrumentation Reference Book embraces the equipment and systems used to detect, track and store data related to physical, chemical, electrical, thermal and mechanical properties of materials, systems and operations. While traditionally a key area within mechanical and industrial engineering, understanding this greater and more complex use of sensing and monitoring controls and systems is essential for a wide variety of engineering areas--from manufacturing to chemical processing to aerospace operations to even the everyday automobile. In turn, this has meant that the automation of manufacturing, process industries, and even building and infrastructure construction has been improved dramatically. And now with remote wireless instrumentation, heretofore inaccessible or widely dispersed operations and procedures can be automatically monitored and controlled. This already well-established reference work will reflect these dramatic changes with improved and expanded coverage of the traditional domains of instrumentation as well as the cutting-edge areas of digital integration of complex sensor/control systems. - Thoroughly revised, with up-to-date coverage of wireless sensors and systems, as well as nanotechnologies role in the evolution of sensor technology - Latest information on new sensor equipment, new measurement standards, and new software for embedded control systems, networking and automated control - Three entirely new sections on Controllers, Actuators and Final Control Elements; Manufacturing Execution Systems; and Automation Knowledge Base - Up-dated and expanded references and critical standards







Basic Concepts Of Analytical Chemistry


Book Description

Analytical Chemistry Has Made Significant Progress In The Last Two Decades. Several Methods Have Come To The Forefront While Some Classical Methods Have Been Relegated. An Attempt Has Been Made In This Edition To Strike A Balance Between These Two Extremes, By Retaining Most Significant Methods And Incorporating Some Novel Techniques. Thus An Endeavour Has Been Made To Make This Book Up To Date With Recent Methods.The First Part Of This Book Covers The Classical Volumetric As Well As Gravimetric Methods Of Analysis. The Separation Methods Are Prerequisite For Dependable Quantitative Methods Of Analysis. Therefore Not Only Solvent Extraction Separations But Also Chromatographic Methods Such As Adsorption, Partition, Ion- Exchange, Exclusion Andelectro Chromatography Have Been Included. To Keep Pace With Modern Developments The Newly Discovered Techniques Such As Ion Chromatography, Super-Critical Fluid Chromatography And Capillary Electrophoresis Have Been Included.The Next Part Of The Book Encompases The Well Known Spectroscopic Methods Such As Uv, Visible, Ir, Nmr, And Esr Techniques And Also Atomic Absorption And Plasma Spectroscopy And Molecular Luminescences Methods. Novel Analytical Techniques Such As Auger, Esca And Photo Accoustic Spectroscopy Of Surfaces Are Also Included.The Final Part Of This Book Covers Thermal And Radioanalytical Methods Of Analysis. The Concluding Chapters On Electroanalytical Techniques Include Potientometry, Conductometry. Coulometry And Voltametry Inclusive Of All Kinds Of A Polarography. The Theme Of On Line Analysis Is Covered In Automated Methods Of Analysis.To Sustain The Interest Of The Reader Each Chapter Is Provided With Latest References To The Monographs In The Field. Further, To Test The Comprehension Of The Subject Each Chapter Is Provided With Large Number Of Solved And Unsolved Problems.This Book Should Be Useful To Those Reads Who Have Requisite Knowledge In Chemistry And Are Majoring In Analytical Chemistry. It Is Also Useful To Practising Chemists Whose Sole Aim Is To Keep Abreast With Modern Developments In The Field.




The Chemical Analysis of Water


Book Description

Information requirements of measurement programmes; Sampling; Basic problems and aims of sampling; Time and frequency of sampling; Overall design of sampling programmes; Procedures for obtaining samples of waters; Preparation, transport, storage, and stability of samples; The nature and importance of errors in analytical results; Random error; Systematic error; Accuracy; Effects of errors on decision making; Need to estimate analytical errors; Estimation and control of the Bias of analytical results; Detailed consideration and assessment of individual sources of Bias; Assessment of the overall Bias of analytical results; Estimation and control of the precision of analytical results; Model of Random errors; Achievement of specified accuracy by a group of laboratories; Types of inter-laboratory studies; Reporting analytical results; Reporting results close to the lower concentration limit of an analytical system; The selection of analytical methods; General precautions in water-analysis laboratories; Analytical techniques; Automatic and on-line analysis; Computers in water analysis; The scope for computing in water analysis and related activities.




Classification and Nomenclature of Electroanalytical Techniques


Book Description

Classification and Nomenclature of Electroanalytical Techniques contains the revised and updated recommendations on electroanalytical classification and nomenclature. This report follows the general lines of its predecessor, but deviates from it in a number of details. The electroanalytical techniques are classified according to the techniques in which neither the electrical double layer nor any electrode reaction need be considered; techniques that involve double-layer phenomena but in which any electrode reactions need not be considered; and techniques involving electrode reactions.