Problems Of Instrumental Analytical Chemistry: A Hands-on Guide


Book Description

The complex field of analytical chemistry requires knowledge and application of the fundamental principles of numerical calculation. Problems of Instrumental Analytical Chemistry provides support and guidance to help students develop these numerical strategies to generate information from experimental results in an efficient and reliable way. Exercises are provided to give standard protocols to follow which address the most common calculations needed in the daily work of a laboratory. Also included are easy to follow diagrams to facilitate understanding and avoid common errors, making it perfect as a hands-on accompaniment to in-class learning.Subjects covered follow a course in analytical chemistry from the initial basics of data analysis, to applications of mass, UV-Vis, infrared and atomic spectrometry, chromatography, and finally concludes with an overview of nuclear magnetic resonance. Intended as a self-training tool for undergraduates in chemistry, analytic chemistry and related subjects, this book is also useful as a reference for scientists looking to brush up on their knowledge of instrumental techniques in laboratories.







Problems of Instrumental Analytical Chemistry (Second Edition)


Book Description

The book is intended as a tool for undergraduate students. As European Universities converged to the EEES Bologna space, the time available for theoretical and practical lessons at the classroom has reduced dramatically. The fundamental principles and basic theory of Analytical Chemistry, are covered by many wonderful textbooks but the numerical part is not so. Although it is true that many of them present some worked examples, the students need more support. Indeed many teachers observed a serious decline in the calculation capabilities of their students.This book is intended to help undergraduate students of Instrumental Analytical Chemistry to develop strategies to generate information from experimental results in an efficient and reliable way. The exercises will provide standard protocols that students can follow to address the most common calculation steps required in laboratory daily work. It is assumed that they will use the hands-on guide after the basic principles of the analytical techniques were presented in their classes. Easy-to-follow diagrams are included to facilitate understanding of the calculations and avoid common errors.As a novelty, QR codes are inserted into the text to offer additional extra information and/or links to reputed websites with additional explanations and/or computer animations. This new feature is a distinctive one, very rare in scientific or teaching-oriented books.




The Essence Of Crystallography


Book Description

'To summarise, Professor Ladd has written a highly engaging text designed to provide the underlying principles of crystal structure determination through X-ray diffraction data. This text would be most appropriate for an early stage postgraduate or researcher interested in learning both the underlying principles of crystallography and gaining some practice with structure-solving software.'Contemporary PhysicsDesigned for those who wish to understand and engage with the principles behind the process of crystal structure determination by X-ray diffraction, this title contains a comprehensive series of chapters, each of which concludes with a set of problems, for which solutions are provided. An ideal resource for senior undergraduates and early-stage postgraduates, The Essence of Crystallography has an accompanying website with programs written for the text, including an interactive simulation of crystal structure determination using prepared intensity data sets.




Orbitals: With Applications In Atomic Spectra (Revised Edition)


Book Description

'Without being an explicitly philosophical treatise Chas McCaw's book delves into some of the deepest and most difficult aspects of atomic physics and chemistry and its underlying quantum mechanical account … One of the many strengths of the book under review is that it takes a rigorous and unflinching look at the necessary mathematical details. In addition, the author, who is the Head of Science at Winchester College in the UK, provides as many as 107 exercises which are interspersed throughout the main text. The detailed solutions are given at the end of the book, over a sequence of about 50 pages.'Foundations of ChemistryOrbitals: With Applications in Atomic Spectra describes atomic orbitals at a level suitable for undergraduates in chemistry. The mathematical treatment is brought to life by many illustrations rendered from mathematical functions (no artists' impressions), including three-dimensional plots of angular functions, showing orbital phase, and contour plots of the wavefunctions that result from orbital hybridisation.This revised edition includes new discussion of the origins of the colour of gold and the 'accidental degeneracy' of the hydrogen atom subshells, a new figure, a new exercise and worked solution, as well as several new references. It also contains current and accurate updates to the old edition.Orbitals extends the key fundamental quantum properties to many-electron atoms, linear combinations of atomic orbitals, simple molecules, delocalised systems and atomic spectroscopy. By focusing on simple model systems, use of analogies and avoiding group theory, results are obtained from initial postulates without the need for sophisticated mathematics. The book explains topics from first principles and guides the reader carefully through the necessary mathematics, supplemented by worked solutions to problems.




Principles Of Nuclear Chemistry


Book Description

Principles of Nuclear Chemistry is an introductory text in nuclear chemistry and radiochemistry, aimed at undergraduates with little or no knowledge of physics. It covers the key aspects of modern nuclear chemistry and includes worked solutions to end of chapter questions.The text begins with basic theories in contemporary physics and uses these to introduce some fundamental mathematical techniques. It relates nuclear phenomena to key divisions of chemistry such as atomic structure, spectroscopy, equilibria and kinetics. It also gives an introduction to f-block chemistry and the nuclear power industry.This book is essential reading for those taking a first course in nuclear chemistry and is a useful companion to other volumes in physical and analytical chemistry. It will also be of use to those new to working in nuclear chemistry or radiochemistry.




Atmospheric Chemistry: From The Surface To The Stratosphere


Book Description

Understanding the composition and chemistry of the Earth's atmosphere is essential to global ecological and environmental policy making and research. Atmospheric changes as a result of both natural and anthropogenic activity have affected many of the Earth's natural systems throughout history, some more seriously than others, and such changes are ever more evident with increases in both global warming and extreme weather events. Atmospheric Chemistry considers in detail the physics and chemistry of our atmosphere, that gives rise to our weather systems and climate, soaks up our pollutants and protects us from solar UV radiation.The development of the complex chemistry occurring on Earth can be explained through application of basic principles of physical chemistry, as is discussed in this book. It is therefore accessible to intermediate and advanced undergraduates of chemistry, with an interdisciplinary approach relevant to meteorologists, oceanographers, and climatologists. It also provides an ideal opportunity to bring together many different aspects of physical chemistry and demonstrate their relevance to the world we live in.This book was written in conjunction with Astrochemistry: From the Big Bang to the Present Day, Claire Vallance (2017) World Scientific Publishing.




Astrochemistry: From The Big Bang To The Present Day


Book Description

'This book could appeal to astronomers interested in interstellar and circumstellar matter who would like to know more about the processes in them from a chemist's perspective in a modern textbook. Overall, I found this book very informative and clearly written …'The Observatory MagazineThe rapidly growing field of astrochemistry focuses on the chemistry occurring in stars, planets, and the interstellar medium, bringing together elements of chemistry, physics, astrophysics, and biology. Astrochemistry describes the chemical history of the Universe, our solar system, and our planet. It explores in some detail the 'alien' chemistry occurring in interstellar gas clouds, the regions where stars and planets are formed, and also looks at the theoretical and experimental methods that allow us to carry out Earth-based studies of astrochemistry.The evolution of the Universe and the complex chemistry occurring both in interstellar space and in the planetary systems that form in these regions is explained primarily in terms of basic principles of physical chemistry. While there is plenty to interest the general reader, this book is aimed at intermediate to advanced undergraduates of chemistry and astrochemistry, highlighting many different aspects of physical chemistry and demonstrating their relevance to the world we live in.This book was written in conjunction with Atmospheric Chemistry: From the Surface to the Stratosphere, Grant Ritchie (2017) World Scientific Publishing.




Nano and Bio-Based Technologies for Wastewater Treatment


Book Description

Presents recent challenges related to new forms of pollution from industries and discusses adequate state-of-the-art technologies capable to remediate such forms of pollution. Over the past few decades the boom in the industrial sector has contributed to the release in the environment of pollutants that have no regulatory status and which may have significant impact on the health of humans and animals. These pollutants also referred to as "emerging pollutants", are mostly aromatic compounds which derive from excretion of pharmaceutical, industrial effluents and municipal discharge. It is recurrent these days to find water treatment plants which no longer produce water that fits the purpose of domestic consumption based on newly established guidelines. This situation has prompted water authorities and researchers to develop tools for proper prediction and control of the dispersion of pollutants in the environment to ensure that appropriate measures are taken to prevent the occurrence of outbreaks due to sudden load of these pollutants in the water system. The chapters in this book cover a wide range of nano and bio-based techniques that have been designed for the real time detection of emerging contaminants in environmental water sources, geochemical models that are continuously improved for the prediction of inorganic contaminants migration from the mine solid wastes into ground and surface waters. Remediation strategies are also discussed and include effective techniques based on nanotechnology, advanced membrane filtration, oxidative and bio-degradation processes using various types of nanocatalysts, biocatalysts or supporting polymer matrices which are under advanced investigations for their implementation at large scale for the removal of recalcitrant pollutants from polluted water. Nano and Bio-Based Technologies for Wastewater Treatment: Prediction and Control Tools for the Dispersion of Pollutants in the Environment is divided is two sections. The first section covers the occurrence of emerging pollutants in environmental water while the second section covers state-of-the-art research on the removal of emerging pollutants from water using sustainable technologies. A total of 13 chapters addressing various topics related to the two sections are essentially based on recent developments in the respective field which could have a significant impact on the enhancement of the performance of wastewater treatment plants around the world, and especially in developing countries where access to clean and safe water remains a daily challenge.




Software-assisted Method Development In High Performance Liquid Chromatography


Book Description

'The book is a useful contribution in the field of HPLC, and may represent a valuable tool for chromatography practitioners in different fields, as well as teachers and instructors. The 12 chapters provide comprehensive insights of current day retention and resolution modelling in HPLC, and its applications for small and large molecule analysis. It may be a useful reference for specialists in pharmaceuticals but not limited to … It may be a valuable resource to assist scientists involved in method development, aiming to achieve the best results with reduced costs, time, and efforts.'Analytical and Bioanalytical ChemistryThis handbook gives a general overview of the possibilities in recent developments in chromatographic retention modeling. As a result of the latest developments in modeling software, several new features are now accessible, opening a new level in HPLC method development.Many of these current possibilities in software assisted liquid chromatographic method modeling for analytical purposes are presented. Several modes of chromatography, including Reversed-Phase Liquid Chromatography (RPLC), Ion Exchange Chromatography (IEX), Hydrophobic Interaction Chromatography (HIC), and Hydrophilic Interaction Liquid Chromatography (HILIC) are explained in detail. For all these chromatographic modes, the most important variables for tuning retention and selectivity are exposed.Beside the industrial and practical benefits of retention modeling, the possibilities in teaching and education are also illustrated. Finally, numerous representative industrial examples are shown, to highlight the benefits, time and cost savings offered by state-of-the-art software assisted HPLC method development.