Thin-Layer Chromatography for Binding Media Analysis


Book Description

In the study and conservation of art and artifacts, natural organic materials are frequently encountered in components such as coatings, binders, and adhesives. The identification of these materials is often crucial to the attempt to characterize the technologies employed by artists or craftspeople, understand the processes and causes of deterioration, and plan appropriate conservation treatments. Yet the limited resources of many conservation laboratories put many analysis techniques beyond their reach. Thin-layer chromatography can help fill this gap. The volume consists of a handbook, protocols, and guide to reference materials. The handbook serves as a primer for the basic application of thin-layer chromatography to the analysis of binding media, adhesives, and coatings found on cultural objects; the protocols provide step-by-step instructions for the laboratory procedures involved in typical analyses; and the guide to reference materials aids in the understanding of the types of materials and documentation needed for accurate analyses by thin-layer chromatography.




Thin Layer Chromatography in Drug Analysis


Book Description

Used routinely in drug control laboratories, forensic laboratories, and as a research tool, thin layer chromatography (TLC) plays an important role in pharmaceutical drug analyses. It requires less complicated or expensive equipment than other techniques, and has the ability to be performed under field conditions. Filling the need for an up-to-date




Instrumental Thin-Layer Chromatography


Book Description

Instrumental Thin-Layer Chromatography, Second Edition offers a comprehensive source of authoritative information on all aspects of instrumental thin-layer chromatography. The use of short, topic-focused chapters facilitates identifying information of immediate interest for familiar or emerging uses of thin-layer chromatography. The book gives those working in both academia and industry the opportunity to learn, refresh, or deepen their understanding of fundamental and instrumental aspects of thin-layer chromatography, as well as the tools to interpret and manage chromatographic data. The book serves as a practical consolidated guide to the selection of separation conditions and the use of auxiliary techniques. This fully updated new edition restores the contemporary character of the book for those involved in advancing the technology, analyzing data produced, or applying the technique to new application areas. Some chapters have been consolidated to make room for topics not covered in the first edition, reflecting general changes in the field of thin-layer chromatography, especially in effects-directed detection, convenient interfaces for advanced spectroscopic detection, and greater automation possibilities. This book is a valuable reference for anyone who needs to acquire fundamental and practical information to facilitate progress in research and management functions utilizing information acquired by thin-layer chromatography. - Features individual chapters written by recognized authoritative and visionary experts in the field - Provides an overview and focused treatment of a single topic - Provides tables and diagrams with commonly used data to facilitate practical work, comparison of results, and decision-making - Places modern developments in the research literature into a general context not always apparent to inexperienced users of the technique - Offers comprehensive updates to all chapters - Includes new chapters on instrument platforms, effects-directed detection, data analysis tools, small-scale and microfluidic planar separation systems, and applications to the separation of amino acids and peptides, the analysis of saccharides and lipids, and forensic analysis




Organic Mass Spectrometry in Art and Archaeology


Book Description

Offers an overview of the analysis of art and archaeological materials using techniques based on mass spectrometry Illustrates basic principles, procedures and applications of mass spectrometric techniques. Fills a gap in the field of application on destructive methods in the analysis of museum objects Edited by a world-wide respected specialists with extensive experience of the GC/MS analysis of art objects Such a handbook has been long-awaited by scientists, restorers and other experts in the analysis of art objects




Planar Chromatography - Mass Spectrometry


Book Description

Planar Chromatography-Mass Spectrometry focuses on a relatively new approach to chemical analysis in general, and to separation science in particular. It is the first book to systemically cover the theoretical background, techniques, instrumentation, and practical applications of planar chromatography-mass spectrometry as a hyphenated tool of analy




Research Abstracts of the Scientific Program


Book Description

This series presents current research being conducted under the auspices of the Getty Conservation Institute.An overview of research from 1984 to 1994, including environmental controls in museums, the use of protective materials and analyses in the conservation of cultural objects and archaeological sites, and the use of new technologies for monitoring, documentation, and analysis.




Historical Textiles and Their Characterization


Book Description

This book utilizes current scientific advances to better understand the principles of degradation of historical textile materials (including ancient mummies, dresses, jewellery and musical instruments) and their characterisation. Moreover, it highlights the importance of multidisciplinary procedures as a part of complex task when only a relatively low amount of materials are available for analysis. In such cases, only sensitive, selective and reliable analytical procedures, such as microscopy, spectroscopy and chromatography, can be applied in the characterization of precious materials. As this book explores current scientific advances to better understand the principles of materials characterisation, it is of broad general interest to the general public, but also to the chemical, anthropological and conservation-restoration communities. Moreover, it also offers particular support to a global audience interested in the preservation of historical materials.




Quantitative Thin-Layer Chromatography


Book Description

Thin-layer chromatography (TLC) is widely used particularly for pharmaceutical and food analysis. While there are a number of books on the qualitative identification of chemical substances by TLC, the unique focus here is on quantitative analysis. The authors describe all steps of the analytical procedure, beginning with the basics and equipment for quantitative TLC followed by sample pretreatment and sample application, development and staining, scanning, and finally statistical and chemometric data evaluation and validation. An important feature is the coverage of effect-directed biological detection methods. Chapters are organized in a modular fashion facilitating the easy location of information about individual procedural steps.




Painted Wood


Book Description

The function of the painted wooden object ranges from the practical to the profound. These objects may perform utilitarian tasks, convey artistic whimsy, connote noble aspirations, and embody the highest spiritual expressions. This volume, illustrated in color throughout, presents the proceedings of a conference organized by the Wooden Artifacts Group of the American Institute for Conservation of Historic and Artistic Works (AIC) and held in November 1994 at the Colonial Williamsburg Foundation in Williamsburg, Virginia. The book includes 40 articles that explore the history and conservation of a wide range of painted wooden objects, from polychrome sculpture and altarpieces to carousel horses, tobacconist figures, Native American totems, Victorian garden furniture, French cabinets, architectural elements, and horse-drawn carriages. Contributors include Ian C. Bristow, an architect and historic-building consultant in London; Myriam Serck-Dewaide, head of the Sculpture Workshop, Institut Royal du Patrimoine Artistique, Brussels; and Frances Gruber Safford, associate curator of American decorative arts at the Metropolitan Museum of Art in New York. A broad range of professionals—including art historians, curators, scientists, and conservators—will be interested in this volume and in the multidisciplinary nature of its articles.




Analytical Techniques in Materials Conservation


Book Description

This book will introduce the reader to the wide variety of analytical techniques that are employed by those working on the conservation of materials. An introduction to each technique is provided with explanations of how data may be obtained and interpreted. Examples and case studies will be included to illustrate how each technique is used in practice. The fields studied include: inorganic materials, polymers, biomaterials and metals. Clear examples of data analysis feature, designed to assist the reader in their choice of analytical method.