Advanced Experimental Inorganic Chemistry


Book Description

This book is divided into four parts: Part I deals with Qualitative Inorganic Analysis. Systematic procedures of anion and cation analysis alongwith their confirmatory tests and spot tests are given. Detection of cations by flame photometry and atomic absorption spectroscopy are also incorporated. Besides chromatographic separation and identification of cations are also discussed Part II deals with volumetric analysis. The instrumental methods of volumetric analysis have also been incorporated Part III deals with gravimetric analysis. Estimation of one or more than one constituent in a solution and instrumental methods of quantitative analysis are also incorporated Part IV describes many inorganic preparations. These include simple salts, double salts, complex salts, amalgams, activated metals, organometallics and some other miscellaneous inorganic preparations. The uses of various compounds have also been mentioned Print edition not for sale in South Asia (India, Sri Lanka, Nepal, Bangladesh, Pakistan or Bhutan)




Synthesis and Technique in Inorganic Chemistry


Book Description

Previously by Angelici, this laboratory manual for an upper-level undergraduate or graduate course in inorganic synthesis has for many years been the standard in the field. In this newly revised third edition, the manual has been extensively updated to reflect new developments in inorganic chemistry. Twenty-three experiments are divided into five sections: solid state chemistry, main group chemistry, coordination chemistry, organometallic chemistry, and bioinorganic chemistry. The included experiments are safe, have been thoroughly tested to ensure reproducibility, are illustrative of modern issues in inorganic chemistry, and are capable of being performed in one or two laboratory periods of three or four hours. Because facilities vary from school to school, the authors have included a broad range of experiments to help provide a meaningful course in almost any academic setting. Each clearly written & illustrated experiment begins with an introduction that hig! hlights the theme of the experiment, often including a discussion of a particular characterization method that will be used, followed by the experimental procedure, a set of problems, a listing of suggested Independent Studies, and literature references.







Understanding Experimental Planning For Advanced Level Chemistry: The Learner's Approach


Book Description

This book is a continuation of authors' previous six books — Understanding Advanced Physical Inorganic Chemistry, Understanding Advanced Organic and Analytical Chemistry, Understanding Advanced Chemistry Through Problem Solving Vol. I & II, Understanding Basic Chemistry and Understanding Basic Chemistry Through Problem Solving, retaining the main refutational characteristics of the previous books with the strategic inclusion of think-aloud questions to promote conceptual understanding during an experimental planning. These essential questions would make learners aware of the rationale behind each procedural step, the amount of chemical used and types of apparatus that are appropriate for the experiment.The book provides a fundamental important scaffolding to aid students to create their own understanding of how to plan an experiment based on the given reagent and apparatus. It guides the students in integrating the various concepts that they have learnt into a coherent and meaningful conceptual network during experimental planning.Existing A-level or IB guidebooks generally introduce concepts in a matter-of-fact manner. This book adds a unique pedagogical edge which few can rival. This book is essential and useful in order for students to be adequately prepared for their high stake examinations.




Understanding Advanced Physical Inorganic Chemistry: The Learner's Approach (Revised Edition)


Book Description

This revised edition has been updated to meet the minimum requirements of the new Singapore GCE A level syllabus that would be implemented in the year 2016. Nevertheless, this book is also highly relevant to students who are studying chemistry for other examination boards. In addition, the authors have also included more Q&A to help students better understand and appreciate the chemical concepts that they are mastering.







Inorganic Experiments


Book Description

Offers detailed descriptions of more than 60 experiments ranging from undergraduate to graduate level, covering organometallic, main group, solid state and coordination chemistry--Cover.




Practical Approaches to Biological Inorganic Chemistry


Book Description

Practical Approaches to Biological Inorganic Chemistry, Second Edition, reviews the use of spectroscopic and related analytical techniques to investigate the complex structures and mechanisms of biological inorganic systems that contain metals. Each chapter presents an overview of the technique, including relevant theory, a clear explanation of what it is, how it works, and how the technique is actually used to evaluate biological structures. New chapters cover Raman Spectroscopy and Molecular Magnetochemistry, but all chapters have been updated to reflect the latest developments in discussed techniques. Practical examples, problems and many color figures are also included to illustrate key concepts. The book is designed for researchers and students who want to learn both the basics and more advanced aspects of key methods in biological inorganic chemistry. - Presents new chapters on Raman Spectroscopy and Molecular Magnetochemistry, as well as updated figures and content throughout - Includes color images throughout to enable easier visualization of molecular mechanisms and structures - Provides worked examples and problems to help illustrate and test the reader's understanding of each technique - Written by leading experts who use and teach the most important techniques used today to analyze complex biological structures




Comprehensive Organic Chemistry Experiments for the Laboratory Classroom


Book Description

This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment. Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students.




Structural Methods in Molecular Inorganic Chemistry


Book Description

Determining the structure of molecules is a fundamental skill that all chemists must learn. Structural Methods in Molecular Inorganic Chemistry is designed to help readers interpret experimental data, understand the material published in modern journals of inorganic chemistry, and make decisions about what techniques will be the most useful in solving particular structural problems. Following a general introduction to the tools and concepts in structural chemistry, the following topics are covered in detail: • computational chemistry • nuclear magnetic resonance spectroscopy • electron paramagnetic resonance spectroscopy • Mössbauer spectroscopy • rotational spectra and rotational structure • vibrational spectroscopy • electronic characterization techniques • diffraction methods • mass spectrometry The final chapter presents a series of case histories, illustrating how chemists have applied a broad range of structural techniques to interpret and understand chemical systems. Throughout the textbook a strong connection is made between theoretical topics and the real world of practicing chemists. Each chapter concludes with problems and discussion questions, and a supporting website contains additional advanced material. Structural Methods in Molecular Inorganic Chemistry is an extensive update and sequel to the successful textbook Structural Methods in Inorganic Chemistry by Ebsworth, Rankin and Cradock. It is essential reading for all advanced students of chemistry, and a handy reference source for the professional chemist.