Reactive and Membrane-Assisted Separations


Book Description

Process intensification aims for increasing efficiency and sustainability of (bio-)chemical production processes. This book presents strategies for improving fluid separation such as reactive distillation, reactive absorption and membrane assisted separations. The authors discuss computer simulation, model development, methodological approaches for synthesis and the design and scale-up of final industrial processes.




Reactive Separation Processes


Book Description

This book summarizes the available information in six known areas of reactive separation: reaction/distillation, reaction/extraction, reaction/absorption, reaction/adsorption, reaction/membrane, and reaction/crystallization.




Process Intensification


Book Description

Intensified processes have found widespread application in the chemical and petrochemical industries. The use of intensified systems allows for a reduction of operating costs and supports the “greening” of chemical processes. However, the design of intensified equipment requires special methodologies. This book describes the fundamentals and applications of these design methods, making it a valuable resource for use in both industry and academia.




Reactive Distillation


Book Description

In a reactive distillation column, both the chemical conversion and the distillative separation of the product mixture are carried out simultaneously. Through this integrative strategy, chemical equilibrium limitations can be overcome, higher selectivities can be achieved and heat of reaction can be directly used for distillation. Increased process efficiency and reduction of investments and operational costs are the direct results of this approach. Highly renowned international experts from both industry and academia review the state-of-the-art and the future directions in application, design, analysis and control of Reactive Distillation processes. Part I surveys various industrial applications and covers both established large scale processes as well as new chemical reaction schemes with high future potential. Part II provides the vital details for analysis of reactive phase equilibria, and discusses the importance of chemical reaction kinetics, while Part III focuses on identifying feasible column configurations and designing their internal structure. Analysis and control of the complex dynamic and steady-state behavior of reactive distillation processes are described in Part IV. Reactive Distillation - a very promising alternative to conventional reaction-distillation flow schemes.




Separation and Purification Technologies in Biorefineries


Book Description

Separation and purification processes play a critical role in biorefineries and their optimal selection, design and operation to maximise product yields and improve overall process efficiency. Separations and purifications are necessary for upstream processes as well as in maximising and improving product recovery in downstream processes. These processes account for a significant fraction of the total capital and operating costs and also are highly energy intensive. Consequently, a better understanding of separation and purification processes, current and possible alternative and novel advanced methods is essential for achieving the overall techno-economic feasibility and commercial success of sustainable biorefineries. This book presents a comprehensive overview focused specifically on the present state, future challenges and opportunities for separation and purification methods and technologies in biorefineries. Topics covered include: Equilibrium Separations: Distillation, liquid-liquid extraction and supercritical fluid extraction. Affinity-Based Separations: Adsorption, ion exchange, and simulated moving bed technologies. Membrane Based Separations: Microfiltration, ultrafiltration and diafiltration, nanofiltration, membrane pervaporation, and membrane distillation. Solid-liquid Separations: Conventional filtration and solid-liquid extraction. Hybrid/Integrated Reaction-Separation Systems: Membrane bioreactors, extractive fermentation, reactive distillation and reactive absorption. For each of these processes, the fundamental principles and design aspects are presented, followed by a detailed discussion and specific examples of applications in biorefineries. Each chapter also considers the market needs, industrial challenges, future opportunities, and economic importance of the separation and purification methods. The book concludes with a series of detailed case studies including cellulosic bioethanol production, extraction of algae oil from microalgae, and production of biopolymers. Separation and Purification Technologies in Biorefineries is an essential resource for scientists and engineers, as well as researchers and academics working in the broader conventional and emerging bio-based products industry, including biomaterials, biochemicals, biofuels and bioenergy.




Process Intensification


Book Description

Process intensification aims for increasing efficiency and sustainability of (bio-)chemical production processes. The second book of our two-book series focusses entirely on process intensifi cation by centrifugally enhanced (reactive) separations. The book provides an overview of the main applications of rotating packed beds (RPBs) in liquid-liquid, gas-liquid and vapor-liquid contacting, within academic research and industrial applications. The book addresses current design rules and modeling frameworks, including the tailored design of functional packings by means of additive manufacturing. Rotating packed beds are widely applicable and fl exible mass transfer machines for process intensifi cation. Applications, design rules and advanced modeling for rotating packed beds are presented in an interconnected way.




Reactive Separation Processes


Book Description

This book summarizes the available information in six known areas of reactive separation: reaction/distillation, reaction/extraction, reaction/absorption, reaction/adsorption, reaction/membrane, and reaction/crystallization.




Reactive Separation for Process Intensification and Sustainability


Book Description

This book describes, analyses and discusses the main principles, phenomena and design strategies of reactive separation processes with an emphasis on the intensification as a basis of the sustainability. Different reactive separation processes are explained in detail to show the phenomena and with the purpose of understanding when their use allows advantages based on the output results. Case examples are analysed and the perspective of these processes in the future is discussed. The overall sustainability of reactive separation processes in the industry is also explained separately.




Distillation: Equipment and Processes


Book Description

Distillation: Equipment and Processes—winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers—is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on distillation equipment and processes. - Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers - Practical information on the newest development written by recognized experts - Coverage of a huge range of laboratory and industrial distillation approaches - Extensive references for each chapter facilitates further study




Process Intensification


Book Description

Process intensifi cation aims for increasing effi ciency and sustainability of (bio-)chemical production processes. This book presents strategies for the intensifi cation of fluid separation processes such as reactive distillation, reactive absorption and membrane assisted separations. The authors discuss theoretical fundamentals, model development, methods for synthesis and the design as well as scale-up and industrial process applications.