High-Temperature Measurements of Materials


Book Description

A variety of industries – information technology, aerospace, automobile, and basic and new materials manufacturing – need technological innovations, which bring high-value-added and high-quality products at low cost not only because of global competition, but also because of the perspective of en- ronmental consciousness and regulation. Thermophysical properties of hi- temperature melts are indispensable for numerical simulations of material processes such as semiconductor and optical crystal growth of the melt, and castingofsuper-high-temperaturealloysforjet-engineturbineblades,inad- tion to welding in automobile manufacturing. Recent developments in process modeling provide 3D unsteady analysis of melt convection, temperature, and heat ?ux distribution, which enables us to predict product quality. In fact, 3D process visualization using computer modeling helps us to understand complicated phenomena occurring in the melt and to control the process. Accurate data are necessary to improve the modeling, which co- e?ectively engenders high-quality products. However, crucial obstacles render measurements of thermophysical properties di?cult at elevated temperatures because of high chemical reactivity and ?uidity of melts. Substantial and persistent challenges have been made to ascertain the precise thermophysical properties of high-temperature melts. This book describes the new techniques and latest developments in the measurements of atomic structure, density, surface tension, viscosity, heat capacity, thermal and mass di?usivity, th- mal conductivity, emissivity, and electrical conductivity of high-temperature melts. In addition to up-to-date improvements in conventional techniques, some new attempts are introduced to open a new scienti?c ?eld, that is, physics of high-temperature melts.




Temperature Measurement


Book Description

Die exakte Temperaturmessung ist ein wichtiger Parameter in vielen Bereichen. Dieser Band wurde komplett überarbeitet und aktualisiert und enthält darüber hinaus die neuesten IEC Standards. Theorie und instrumentelle Praxis der Temperaturbestimmung werden hier umfassend behandelt. (09/00)




Practical Temperature Measurement


Book Description

Temperature * General temperature measurement considerations * Invasive temperature measurement * Semi-invasive temperature measurement * Non-invasive temperature measurement * Temperature measurement technique selection * Heat flux measurement * Conclusions.




Research Techniques for High Pressure and High Temperature


Book Description

Within the last two decades, the experimental technology for the study of high temperature solid-vapor and liquid-vapor equilibria has mushroomed so fast that· both academic and industrial research ers desirous of working in this field -- be they physical chemists, metallurgists, ceramists, petrologists, crystal chemists, or mem bers of any of the several branches of materials science -- find themselves in the situation that in order to learn the art of the latest techniques, a period of apprenticeship or residency needs be spent at an institution or laboratory currently engaged in this type of solid-vapor or liquid-vapor research. The tech niques for control of the vapor phase at total pressures of one atmosphere or greater have not been well defined in the literature. Therefore, the purpose of this volume will be to serve as a labora tory manual for the control, calibration, and measurement of high temperature-high pressure equilibria. The avowed aims of this treatment of experimental techniques are: (1) to give, in terms understandable at the graduate student level, the laboratory procedures necessary to the design and utilization of good experimental technique, (2) to list the limitations, dangers, and technical pitfalls inherent or intrinsic to the described techniques, (3) to give theory and specific data only where they are essential to the experimental design, (4) to give with each chapter references that are extensive enough to serve as a bibliography of the state-of-the-art of technique development within the last decade.







High-Temperature Superconductivity in Cuprates


Book Description

The main purpose of the book is to present a description of the mechanism of high-temperature superconductivity and to discuss the physics of high-temperature superconductors, both entirely based on experimental facts. The pairing mechanism of this remarkable phenomenon is based on an anomaly found in tunneling (V) characteristics of some cuprates. By using the soliton theory, it is then shown that this anomaly is caused by pairs of quasi-one dimensional excitations - bisolitons - bound due to a moderately strong, nonlinear electron-phonon interaction. At the same time, analysis of experimental data unambiguously shows that magnetic (spin) fluctuations mediate the phase coherence in cuprates. The mechanism of superconductivity in quasi-one dimensional organic superconductors and heavy fermions is discussed too. In cuprates, the origins of five different energy/temperature scales are identified. Finally, three main principles of superconductivity are introduced at the end of the book. Analysis of tunneling and angle-resolved photoemission measurements is presented in the last chapter. The book which contains 300 pages with 180 illustrations is addressed to researchers and graduate students in all branches of exact sciences.







Radiometric Temperature Measurements


Book Description

This book describes the practice of radiation thermometry, both at a primary level and for a variety of applications, such as in the materials processing industries and remote sensing. This book is written for those who will a) apply radiation thermometry in industrial practice b) use radiation thermometers for scientific research, c) the radiation thermometry specialist in a national measurement institute d) developers of radiation thermometers who are working to innovate products for instrument manufacturers and e) developers non-contact thermometry methods to address challenging thermometry problems. The author(s) of each chapter were chosen from a group of international scientists who are experts in the field and specialist(s) on the subject matter covered in the chapter. A large number of references are included at the end of each chapter as a resource for those seeking a deeper or more detailed understanding. This book is more than a practice guide. Readers will gain in-depth knowledge in: (1) the proper selection of the type of thermometer; (2) the best practice in using the radiation thermometers; (3) awareness of the error sources and subsequent appropriate procedure to reduce the overall uncertainty; and (4) understanding of the calibration chain and its current limitations. - Coverage of all fundamental aspects of the radiometric measurements - Coverage of practical applications with details on the instrumentation, calibration, and error sources - Authors are from the national labs internationally leading in R&D in temperature measurements - Comprehensive coverage with large number of references







High Temperature Experiments in Chemistry and Materials Science


Book Description

Cutting edge high temperature materials include high temperature superconductors, solid oxide fuel cells, thermoelectric materials and ultrahigh temperature construction materials (including metals, cermets and ceramics) and have applications in key areas such as energy, transportation and space technologies. This book introduces the concepts which underpin research into these critical materials including thermodynamics, kinetics and various physical, chemical and modelling techniques with a focus on practical “how to” methods and covers: Introduction to High Temperature Research Basic Design of High Temperature Furnaces Temperature Measurement Radiation Pyrometry Refractory Materials in the Laboratory Vacuum in Theory and Practice The Design of Vacuum Furnaces and Thermobalances With highly detailed instrument illustrations and an emphasis on the control and measurement of the fundamental properties of temperature, pressure and mass, High Temperature Experiments in Chemistry and Materials Science provides a practical reference on high temperature measurements, for researchers, advanced students and those working in academic or industrial laboratories. Introduction to High Temperature Research Basic Design of High Temperature Furnaces Temperature Measurement Radiation Pyrometry Refractory Materials in the Laboratory Vacuum in Theory and Practice The Design of Vacuum Furnaces and Thermobalances