Cracks in superalloys


Book Description

Gas turbines are widely used in industry for power generation and as a power source at hard to reach locations where other possibilities for electrical power supplies are insufficient. New ways of producing greener energy is needed to reduce emission levels. This can be achieved by increasing the combustion temperature of gas turbines. High combustion temperatures can be detrimental and degrade critical components. This raises the demands on the high temperature performance of the superalloys used in gas turbine components. These components are frequently subjected to different cyclic loads combined with for example dwell-times and overloads at elevated temperatures, which can influence the crack growth. Dwell-times have been shown to accelerate crack growth and change cracking behaviour in both Inconel 718, Haynes 282 and Hastelloy X. On the other hand, overloads at the beginning of a dwell-time cycle have been shown to retard the dwell-time effect on crack growth in Inconel 718. More experiments and microstructural investigations are needed to better understand these effects. The work presented in this thesis was conducted under the umbrella of the research program Turbo Power; "High temperature fatigue crack propagation in nickel-based superalloys", where I have mainly looked at fatigue crack growth mechanisms in superalloys subjected to dwell-fatigue, which can have a devastating effect on crack propagation behaviour. Mechanical testing was performed under operation-like cycles in order to achieve representative microstructures and material data for the subsequent microstructural work. Microstructures were investigated using light optical microscopy and scanning electron microscopy (SEM) techniques such as electron channeling contrast imaging (ECCI) and electron backscatter diffraction (EBSD). The outcome of this work has shown that there is a significant increase in crack growth rate when dwell-times are introduced at maximum load (0 % overload) in the fatigue cycle. With the introduction of a dwell-time there is also a shift from transgranular to intergranular crack growth for both Inconel 718 and Haynes 282. The crack growth rate decreases with increasing overload levels in Inconel 718 when an overload is applied prior to the dwell-time. At high temperature, intergranular crack growth was observed in Inconel 718 as a result of oxidation and the creation of nanometric voids. Another observed growth mechanism was crack advance along ?-phase boundaries with subsequent oxidation of the ?-phase. This thesis comprises two parts. Part I gives an introduction to the field of superalloys and the acting microstructural mechanisms related to fatigue and crack propagation. Part II consists of five appended papers, which report the work completed as part of the project.




Threshold Crack Growth Behavior of Nickel-Base Superalloy at Elevated Temperature


Book Description

An experimental program was conducted to evaluate the effects of frequency and R on the near-threshold crack growth behavior of Inconel 718 at 649°C in laboratory air. Frequencies from 0.01 to 400 Hz and R from 0.1 to 0.9 were applied to compact tension [C(T)] and middle- or center-cracked tension [M(T)] specimens under decreasing-K conditions using computer-controlled test machines. Digital load-displacement data were obtained to determine crack length and closure load. The fatigue crack growth threshold in Inconel 718 at 649°C obtained using decreasing ?K testing was generally associated with a crack arrest phenomenon which could be attributed to the buildup of oxides with time. Over the ranges of R and v used in this investigation, the growth rate behavior at the onset of crack arrest appears to be a combination of time-dependent and cyclic-dependent behavior. Even at 400 Hz, purely cyclic behavior was apparently never reached. For crack growth rate modeling, both frequency and stress ratio have to be incorporated in the characterization of ?Kth. Over the ranges of parameters tested, a cyclic threshold was approached at high frequencies and low R and a sustained load time-dependent threshold was obtained at high R, indicating that the cyclic contribution to the growth rate was negligible.




Near-Threshold Crack Growth in Nickel-Base Superalloys


Book Description

The influence of stress ratio on the elevated-temperature crack growth behavior of the nickel-base superalloys René 95 and Alloy 718 is discussed. The near-threshold and Region II crack growth behavior of a wide variety of microstructures for each alloy are explained using phenomenological descriptions of closure, that is, K-dependent or K-independent closure. K-dependent closure is the type of closure observed for nickel-base superalloys where increasing the R-ratio causes a uniform lateral shift of the entire fatigue crack growth curve. K-independent closure is the type commonly reported for steels and titanium alloys where increasing the R-ratio has a larger influence on near-threshold crack growth than on Region II crack growth. The existence of K-dependent closure in nickel-base superalloys results in microstructurally sensitive crack growth rates, even at high R-ratios. This permits the use of K-based crack growth prediction techniques and simplifies alloy and process development for applications having complex loading spectra.







Aspects of Crack Growth in Single-Crystal Nickel-Base Superalloys


Book Description

This Licentiate of Engineering thesis is a product of the results generated in the research project KME-702, which comprises modelling, microstructure investigations and material testing of cast nickel-base superalloys. The main objective of this work is to model the fatigue crack propagation behaviour in single-crystal nickel-base superalloys. To achieve this, the influence of the crystal orientations on the cracking behaviour is assessed. The results show that the crystal orientation is strongly affecting the material response and must be accounted for. Furthermore, a linear elastic crack driving force parameter suitable for describing crystallographic cracking has been developed. This parameter is based on resolved anisotropic stress intensity factors and is able to predict the correct crystallographic cracking plane after a transition from a Mode I crack. Finally, a method to account for inelastic deformations in a linear elastic fracture mechanics context was investigated. A residual stress field is extracted from an uncracked finite-element model with a perfectly plastic material model and superimposed on the stress field from the cracked model with a linear elastic material model to account for the inelastic deformations during the determination of the crack driving force. The modelling work is validated by material testing on two different specimen geometries at different temperatures. This Licentiate of Engineering thesis consists of two parts, where Part I gives an introduction and background to the research area, while Part II consists of three papers. Denna licentiatavhandling är en produkt av resultat som genererats i forskningsprojektet KME-702, och omfattar modellering, mikrostrukturundersökningar och materialprovning av gjutna nickelbaserade superlegeringar. Huvudsyftet med detta arbete är att modellera sprickförloppet under utmattning i enkristallina nickelbaserade superlegeringar. För att uppnå detta har kristallorienteringens inverkan på sprickbeteendet utvärderats. Resultaten visar att kristallorienteringen har en stark inverkan på materialbeteendet, således måste hänsyn till denna tas. Dessutom har en linjär-elastisk sprickdrivkraftsparameter lämplig att beskriva kristallografisk sprickbildning utvecklats. Denna parameter är baserad på anisotropa spänningsintensitetsfaktorer på kristallplan och kan prediktera det korrekta kristallografiska sprickplanet efter övergång från Modus I spricka. Slutligen har undersökts en metod för att ta hand om inelastiska deformationer i en linjär-elastisk brottmekanikskontext. Ett restspänningsfält extraherades från en osprucken finita element modell med en ideal plastisk materialmodell. Denna överlagrades på spänningsfältet från den spruckna modellen, som analyserades med en linjär-elastisk materialmodell, för att ta hänsyn till de inelastiska deformationerna vid bestämning av sprickdrivkraften. Modelleringsarbetet validerades genom materialprovning på två olika provgeometrier vid olika temperaturer. Licentiatavhandlingen består av två delar, där del I ger en introduktion och bakgrund till forskningsområdet medan del II består av tre papper. Dieses Lizentiat der Ingenieurwissenschaften ist im Rahmen des Forschungsprojekts KME-702 entstanden, welches Modellierung, Mikrostrukturuntersuchungen und Materialtests von gegossenen nickelbasierten Superlegierungen umfasst. Das Hauptziel dieser Arbeit ist die Modellierung der Ermüdungsrissausbreitung in einkristallinen nickelbasierten Superlegierungen. Um dieses zu erreichen, wurde der Einfluss der Kristallorientierungen auf das Rissverhalten untersucht. Die Ergebnisse zeigen, dass die Kristallorientierung das Materialverhalten stark beeinflusst und daher berücksichtigt werden muss. Darüber hinaus wurde ein linear elastischer Rissantriebskraftparameter entwickelt, der zum Beschreiben von kristallographischen Rissen geeignet ist. Dieser Parameter basiert auf aufgelösten anisotropen Spannungsintensitätsfaktoren und ist in der Lage, die korrekte kristallographische Rissebene nach einem Übergang von einem Modus I Riss vorherzusagen. Abschließend wird in einem linear-elastisch bruchmechanischen Kontext eine Methode untersucht, die nichtelastischen Deformationen bei der Bestimmung der Rissantriebskraft zu berücksichtigen. Dazu wird aus einem Finite-Elemente Modell, welches keinen Riss aufweist und mit einem perfekt plastischen Materialmodell beschrieben wird, das Restspannungsfeld extrahiert und dem Spannungsfeld überlagert, welches aus dem Modell mit Riss unter Verwendung eines linear elastischen Materialmodells erzeugt wurde. Die Modellierung wird durch Materialtests an zwei verschiedenen Probengeometrien bei unterschiedlichen Temperaturen validiert. Dieses Lizentiat der Ingenieurwissenschaften besteht aus zwei Teilen, wobei Teil I eine Einführung und einen Hintergrund in das Forschungsgebiet gibt, während Teil II aus drei Forschungsartikeln besteht.




Modelling of Crack Growth in Single-Crystal Nickel-Base Superalloys


Book Description

This dissertation was produced at the Division of Solid Mechanics at Linköping University and is part of a research project, which comprises modelling, microstructure investigations and material testing of cast nickel-base superalloys. The main objective of this work was to deepen the understanding of the fracture behaviour of single-crystal nickel-base superalloys and to develop a model to predict the fatigue crack growth behaviour. Frequently, crack growth in these materials has been observed to follow one of two distinct cracking modes; Mode I like cracking perpendicular to the loading direction or crystallographic crack growth on the octahedral {111}-planes, where the latter is associated with an increased fatigue crack growth rate. Thus, it is of major importance to account for this behaviour in component life prediction. Consequently, a model for the prediction of the transition of cracking modes and the correct active crystallographic plane, i.e. the crack path, and the crystallographic crack growth rate has been developed. This model is based on the evaluation of appropriate crack driving forces using three-dimensional finite-element simulations. A special focus was given towards the influence of the crystallographic orientation on the fracture behaviour. Further, a model to incorporate residual stresses in the crack growth modelling is presented. All modelling work is calibrated and validated by experiments on different specimen geometries with different crystallographic orientations. This dissertation consists of two parts, where Part I gives an introduction and background to the field of research, while Part II consists of six appended papers. Die vorliegende Dissertation wurde in der Abteilung für Festigkeitslehre an der Universität von Linköping erstellt und ist Teil eines Forschungsprojektes, welches Modellierung, Mikrostrukturuntersuchungen und Materialtests von gegossenen nickelbasierten Superlegierungen umfasst. Das Hauptziel dieser Arbeit war es, das Verständnis des Bruchverhaltens von einkristallinen Superlegierungen auf Nickelbasis zu vertiefen und ein Modell zur Vorhersage des Wachstumsverhaltens von Ermüdungsrissen zu entwickeln. Es wurde beobachtet, dass das Risswachstum in diesen Materialien einem von zwei unterschiedlichen Rissmodi folgt; Modus I Rissfortschritt senkrecht zur Belastungsrichtung oder kristallographisches Risswachstum auf den oktaedrischen f111g-Ebenen, wobei letzteres mit einer erhöhten Ermüdungsrisswachstumsrate verbunden ist. Somit ist es von grosser Bedeutung dieses Verhalten in der Lebensdauervorhersage einer Komponente zu berücksichtigen. Demzufolge wurde ein Modell für die Vorhersage des Übergangs zwischen den Rissmodi und der korrekten aktiven kristallographischen Ebene, d.h. des Risspfades, sowie der kristallographischen Risswachstumsrate erarbeitet. Dieses Modell basiert auf geeigneten Rissantriebskräften, welche mit Hilfe dreidimensionaler Finite-Elemente-Simulationen berechnet werden. Im Fokus stand insbesondere der Einuss der kristallographischen Orientierung auf das Bruchverhalten. Ausserdem wird ein Modell zur Berücksichtigung von Restspannungen in der Risswachstumsmodellierung präsentiert. Alle Modellierungsarbeiten wurden durch Experimente an verschiedenen Probengeometrien mit unterschiedlichen kristallographischen Orientierungen kalibriert und validiert. Diese Dissertation besteht aus zwei Teilen, wobei Teil I aus einer Einführung und einem Hintergrund in das Forschungsgebiet und Teil II aus sechs beigefügten Forschungsartikeln besteht.




Fracture Mechanics


Book Description







Effect of Frequency on Fatigue Crack Growth Rate of Inconel 718 at High Temperature


Book Description

Fatigue crack growth was studied at 650 deg. C as a function of frequency for several ratios of minimum-to-maximum stress intensity, and for two values of maximum stress intensity factor. Crack lengths were monitored at low frequencies from compliance calculations based on crack mouth opening displacement measurements. At higher frequencies, crack length was measured using a d.c. electric potential system. It was found that fatigue crack growth rate can be characterized in three distinct frequency regions. These three regions represent fully cycle dependent, mixed, and fully time dependent crack growth behavior and each region can be modeled by a power law function. Observation of micro mechanisms support the existence of these three different regions of crack growth. Keywords: Fatigue crack growth, Time dependent growth, Cyclic-dependent growth, Nickel base superalloy, Crack growth rate model, Frequency effects.