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Inorganic Ultramicroanalysis

Author : I. P. Alimarin

Publisher : Elsevier

Page : 168 pages

File Size : 46,23 MB

Release : 2013-10-22

Category : Science

ISBN : 1483150488

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Book Description

Inorganic Ultramicroanalysis focuses on the techniques and experimental methods used in ultramicroanalysis of inorganic compounds. Topics covered include the general apparatus used in the ultramicromethod of chemical analysis, qualitative and quantitative analysis, and methods of separation. This book consists of six chapters and opens with a review of the special features of the ultramicromethod of chemical analysis, paying particular attention to the use of the law of errors to calculate the limiting quantity of a substance necessary for the performance of chemical operations. The surface area of unit volume in the macro- and ultramicromethods of analysis is also compared. The next chapter deals with the general apparatus used in ultramicroanalysis, including the microscope and micromanipulators, and describes techniques of working with small volumes. The reader is then introduced to qualitative and quantitative analysis and methods of separation such as precipitation and electrolysis. The last chapter discusses future prospects for inorganic ultramicroanalysis. This monograph is written primarily for inorganic and analytical chemists.



Spot Tests in Inorganic Analysis

Author : F. Feigl

Publisher : Elsevier

Page : 700 pages

File Size : 23,3 MB

Release : 2012-12-02

Category : Science

ISBN : 0444597980

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Book Description

Many years have passed since the last edition of the present book was published. The discovery during this period of many new reagents has resulted in a vast accumulation of data on their application and made this completely revised edition necessary.Numerous new tests and various new chapters have been added. Chapters 3,4 and 5 of the fifth edition have been combined into one chapter, which is divided into sections devoted to the elements. These sections are arranged in alphabetical order to make for easier location of information on a given element. To further improve the usefulness of the volume, a reference list has been provided for each sub-section followed by a biography of the appropriate quantitative methods.



Organic Reagents in Metal Analysis

Author : K. Burger

Publisher : Elsevier

Page : 269 pages

File Size : 47,96 MB

Release : 2013-10-22

Category : Science

ISBN : 1483160262

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Book Description

International Series of Monographs in Analytical Chemistry, Volume 54: Organic Reagents in Metal Analysis focuses on the factors determining the analytical selectivity of complexation reactions. This book consists of three chapters. Chapter 1 deals with the effects of stability and electronic structure of complexes and formation of mixed ligand complexes on analytical selectivity. The analytical procedures for the accomplishment of many metal analytical tasks are reviewed in Chapter 2. The last chapter provides a tabulated data that facilitates experimental work in the field of metal analysis. This volume is useful to practical analysts and researchers engaged with developments in the field of analytical chemistry and routine metal analyses.





Chemical Analysis of Additives in Plastics

Author : T. R. Crompton

Publisher : Elsevier

Page : 381 pages

File Size : 42,67 MB

Release : 2016-07-29

Category : Technology & Engineering

ISBN : 1483278794

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Book Description

International Series in Analytical Chemistry, Volume 46: Chemical Analysis of Additives in Plastics, Second Edition brings together numerous investigations on the characterization, identification, and determination of various types of additives in plastics. This book is divided into five chapters. Chapters 1 and 2 describe first the methods for examining additives present in polymers based on either direct spectroscopy of a cast polymer film or on solvent extraction of total additives from the polymer followed by quantitative chemical or physical analysis for various components in the extract. Chapter 3 discusses the application of thin-layer and column chromatography to the separation and determination of known additives. Chapters 4 and 5 examine the application of combined chromatographic and spectroscopic techniques for the separation and determination of unknown plastics additives. This book will prove useful to plastics manufacturers, researchers, institutions, and universities.



Isotope Dilution Analysis

Author : J. Tölgyessy

Publisher : Elsevier

Page : 197 pages

File Size : 20,54 MB

Release : 2013-10-22

Category : Science

ISBN : 1483160920

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Book Description

International Series of Monographs in Analytical Chemistry, Volume 49: Isotope Dilution Analysis focuses on the method of isotope dilution analysis (IDA). The book first discusses the principles, types, and theory of IDA. Classification of the methods of IDA; precision, accuracy, and sensitivity of IDA; and types of IDA are described. The text also examines experimental techniques, separation, and mass determination. The separation of components, reagents and tracers, and amount of substance separated are underscored. The text takes a look at the inorganic applications of IDA, including determination of elements and selected procedures. The text examines the applications of IDA in organic chemistry and biochemistry, particularly in the analysis of alcohols and ethers, steroids, penicillin, proteins and amino acids, and insecticides. The book discusses IDA with stable isotopes. Methods for the determination of isotopic composition, fundamentals and technique, and practical applications are underscored. The text also emphasizes the special applications of isotope dilution. Determination of the content of isotopic carriers in radioactive preparations; determination of the coefficient of self-absorption and specific activity; and determination of radioactive contaminants are discussed. The text is a vital reference for readers interested in isotope dilution analysis.



Analytical Chemistry of Organic Halogen Compounds

Author : L. Mázor

Publisher : Elsevier

Page : 292 pages

File Size : 30,19 MB

Release : 2013-09-03

Category : Science

ISBN : 1483160653

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Book Description

Analytical Chemistry of Organic Halogen Compounds presents the procedures applied in the analysis of organic halogen compounds. This book is composed of eight chapters that discuss the methods involved in the production and application of organic halogen compounds and in overcoming contamination problems caused by these compounds. After briefly dealing with the preparation, characteristics, and reactions of organic halogen compounds, this book goes on discussing the fundamental concepts of methods for the detection of halogens in organic compounds, namely, chlorine, bromine, iodine, and fluorine. The following chapter describes the characteristic features, advantages, and disadvantages of ultramicro and submicro chemical methods. A chapter also examines the qualitative and quantitative studies of organic halogen compounds based on the thermal and chemical stability of these compounds. The concluding chapters discuss the interference or interfering effects of halogens and their elimination in the determination of other elements. A list of physical constants of organic halogen compounds of general pharmaceutical and industrial significance is provided. This book is an ideal source for analytical chemists and other workers who are interested in the theoretical bases of the methods.



The Destruction of Organic Matter

Author : T. T. Gorsuch

Publisher : Elsevier

Page : 161 pages

File Size : 25,91 MB

Release : 2013-10-22

Category : Science

ISBN : 1483160882

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Book Description

International Series of Monographs in Analytical Chemistry, Volume 39: The Destruction of Organic Matter focuses on the identification of trace elements in organic compounds. The monograph first offers information on the processes involved in the determination of trace elements in organic matters, as well as the methods not involving complete destruction of these elements. The text surveys the sources of errors in the processes responsible in pinpointing elements in organic compounds. These processes include sampling, disruption of the samples, manipulation, and measurements. The book examines the processes of wet and dry oxidation, including their applications to sulfuric, nitric, and perchloric acids and hydrogen peroxide. The methods of dry ashing and oxidation with excited oxygen and oxidative fusion are elaborated. The text also underscores the varying methods in removing trace elements in organic compounds. The elements include zinc, copper, silver, gold, lead, germanium, titanium, arsenic, bismuth, and vanadium. The book also describes wet digestion methods and dry ashing procedures in the removal of trace elements in organic matters. The monograph is a vital source of information for readers interested in the identification of trace elements in organic compounds.



Enzymatic Methods of Analysis

Author : George G. Guilbault

Publisher : Elsevier

Page : 367 pages

File Size : 12,12 MB

Release : 2013-10-22

Category : Science

ISBN : 1483150542

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Book Description

Enzymatic Methods of Analysis attempts to cover all the aspects of modern enzymatic analysis. Enzymes possess a great potential usefulness in analytical chemistry. The specificity of enzymes can solve the primary problem of most analytical chemists—the analysis of one substance in the presence of many similar compounds that interfere in the analysis. The book begins with two introductory chapters devoted to general considerations of enzymes as reagents and methods of analysis of enzymatic reactions. The next four chapters deal with methods for the assay of specific enzymes, and substrate, activator, and inhibitor analysis using enzymes. In the last two chapters the immobilization of enzymes and the automation of enzymatic reactions are discussed. In addition, a listing of all commercially available enzymes is given in an appendix. It is hoped that the information presented will prove interesting and stimulating to all individuals engaged in research and development.



Substoichiometry in Radiochemical Analysis

Author : Jaromír Růžička

Publisher : Elsevier

Page : 165 pages

File Size : 18,10 MB

Release : 2013-10-22

Category : Science

ISBN : 1483184129

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Book Description

Substoichiometry in Radiochemical Analysis considers application of simple chemistry than the use of complicated instrumentation in studying radiochemical analysis. This book is divided into nine chapters; the first chapter gives an introduction to the content of this monograph. This text then examines the neutron-activation and isotope-dilution analyses, complemented with the general technique and preliminary experiments. Specifically, this book provides the methods for the substoichiometric determination of traces of various elements by the neutron-activation and isotope-dilution analyses. Copper, mercury, gallium, gold, and zinc are some of the elements featured in this particular topic. This topic is followed by the discussion on the analysis of radioactive materials. This text also tackles the automation and comparison with other radiometric methods of substoichiometric analysis, as well as trends in substoichiometry. This book will be helpful for those concerned with substoichiometry, especially those who need a book that presents non-complicated study of the subject.