Laboratory Techniques in Electroanalytical Chemistry, Second Edition, Revised and Expanded


Book Description

This volume provides a practical, intuitive approach to electroanalytical chemistry, presenting fundamental concepts and experimental techniques without the use of technical jargon or unnecessarily extensive mathematics. This edition offers new material on ways of preparing and using microelectrodes, the processes that govern the voltammetric behavior of microelectrodes, methods for characterizing chemically modified electrodes, electrochemical studies at reduced temperatures, and more. The authors cover such topics as analog instrumentation, overcoming solution resistance with stability and grace in potentiostatic circuits, conductivity and conductometry, electrochemical cells, carbon electrodes, film electrodes, microelectrodes, chemically modified electrodes, mercury electrodes, and solvents and supporting electrolytes.




Laboratory Techniques in Electroanalytical Chemistry


Book Description

This volume provides a practical, intuitive approach to electroanalytical chemistry, presenting fundamental concepts and experimental techniques without the use of technical jargon or unnecessarily extensive mathematics. This edition offers new material on ways of preparing and using microelectrodes, the processes that govern the voltammetric behavior of microelectrodes, methods for characterizing chemically modified electrodes, electrochemical studies at reduced temperatures, and more. The authors cover such topics as analog instrumentation, overcoming solution resistance with stability and grace in potentiostatic circuits, conductivity and conductometry, electrochemical cells, carbon electrodes, film electrodes, microelectrodes, chemically modified electrodes, mercury electrodes, and solvents and supporting electrolytes.




Laboratory Techniques in Electroanalytical Chemistry, Revised and Expanded


Book Description

This volume provides a practical, intuitive approach to electroanalytical chemistry, presenting fundamental concepts and experimental techniques without the use of technical jargon or unnecessarily extensive mathematics. This edition offers new material on ways of preparing and using microelectrodes, the processes that govern the voltammetric behavior of microelectrodes, methods for characterizing chemically modified electrodes, electrochemical studies at reduced temperatures, and more. The authors cover such topics as analog instrumentation, overcoming solution resistance with stability and grace in potentiostatic circuits, conductivity and conductometry, electrochemical cells, carbon electrodes, film electrodes, microelectrodes, chemically modified electrodes, mercury electrodes, and solvents and supporting electrolytes.










Analytical Electrochemistry


Book Description

The critically acclaimed guide to the principles, techniques, and instruments of electroanalytical chemistry-now expanded and revised Joseph Wang, internationally renowned authority on electroanalytical techniques, thoroughly revises his acclaimed book to reflect the rapid growth the field has experienced in recent years. He substantially expands the theoretical discussion while providing comprehensive coverage of the latest advances through late 1999, introducing such exciting new topics as self-assembled monolayers, DNA biosensors, lab-on-a-chip, detection for capillary electrophoresis, single molecule detection, and sol-gel surface modification. Along with numerous references from the current literature and new worked-out examples, Analytical Electrochemistry, Second Edition offers clear, reader-friendly explanations of the fundamental principles of electrochemical processes as well as important insight into the potential of electroanalysis for problem solving in a wide range of fields, from clinical diagnostics to environmental science. Key topics include: The basics of electrode reactions and the structure of the interfacial region Tools for elucidating electrode reactions and high-resolution surface characterization An overview of finite-current controlled potential techniques Electrochemical instrumentation and electrode materials Principles of potentiometric measurements and ion-selective electrodes Chemical sensors, including biosensors, gas sensors, solid-state devices, and sensor arrays




Fundamentals of Electroanalytical Chemistry


Book Description

This thoroughly updated open learning text provides an introduction to electroanalytical chemistry, one of today's fastest growing and most exciting frontiers of analytical science. The author discusses electroanalysis in a non-mathematical and informal tutorial style and offers over 250 discussion and self-assessment questions. In addition he includes 50 worked examples that provide excellent material for testing the reader's understanding of the subject matter. The topics covered include the following: * Simple emf measurements with cells * Equilibrium and dynamic measurements * Polarography * Cyclic voltammetry * Rotated disc, ring-disc and wall-jet electrodes * In situ spectroelectrochemistry measurements * Impedance analysis * Preparation of electrodes * Data processing The book also contains a comprehensive bibliography and details of web-based resources. It assumes no prior knowledge of this powerful branch of analytical science and will be an invaluable aid for anyone wanting to perform analytical measurements using electrochemical technqiues. Is approach makes it also ideal for students.




Electroanalytical Techniques in Clinical Chemistry and Laboratory Medicine


Book Description

Dieser praxisbezogene Überblick über alle in der klinischen Chemie und Labormedizin eingesetzten elektroanalytischen Verfahren ist derzeit das einzige umfassende Werk zu diesem Thema auf dem Markt. Der Autor stellt die theoretischen Grundlagen vor und verdeutlicht an zahlreichen Beispielen Umfang und Möglichkeiten des Einsatzes elektroanalytischer Verfahren. Einige Stichworte zum Inhalt sind: Prinzipien und bioanalytische Anwendung von Voltametrie und Potentiometrie, elektrochemische Biosensoren sowie in-vivo Elektrochemie. Das Buch eignet sich gut als Einstieg in das Gebiet, bietet aber auch dem erfahrenen 'Elektroanalytiker' viele Hilfestellungen und Ratschläge.




Laboratory Methods in Dynamic Electroanalysis


Book Description

Laboratory Methods in Dynamic Electroanalysis is a useful guide to introduce analytical chemists and scientists of related disciplines to the world of dynamic electroanalysis using simple and low-cost methods. The trend toward decentralization of analysis has made this fascinating field one of the fastest-growing branches of analytical chemistry. As electroanalytical devices have moved from conventional electrochemical cells (10-20 mL) to current cells (e.g. 5-50 mL) based on different materials such as paper or polymers that integrate thick- or thin-film electrodes, interesting strategies have emerged, such as the combination of microfluidic cells and biosensing or nanostructuration of electrodes. This book provides detailed, easy procedures for dynamic electroanalysis and covers the main trends in electrochemical cells and electrodes, including microfluidic electrodes, electrochemical detection in microchip electrophoresis, nanostructuration of electrodes, development of bio (enzymatic, immuno, and DNA) assays, paper-based electrodes, interdigitated array electrodes, multiplexed analysis, and combination with optics. Different strategies and techniques (amperometric, voltammetric, and impedimetric) are presented in a didactic, practice-based way, and a bibliography provides readers with additional sources of information. Provides easy-to-implement experiments using low-cost, simple equipment Includes laboratory methodologies that utilize both conventional designs and the latest trends in dynamic electroanalysis Goes beyond the fundamentals covered in other books, focusing instead on practical applications of electroanalysis




Electroanalytical Methods


Book Description

This laboratory book delivers hands-on advice to researchers in all fields of life and physical sciences already applying or intending to apply electro-analytical methods in their research. The authors represent in a strictly practice-oriented manner not only the necessary theoretical background but also substantial know-how on measurement techniques, interpretation of data, experimental setup and trouble shooting. The author and the editor are well-known specialists in their field.