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Microreactors in Preparative Chemistry

Author : Wladimir Reschetilowski

Publisher : John Wiley & Sons

Page : 351 pages

File Size : 46,76 MB

Release : 2013-09-13

Category : Science

ISBN : 3527652914

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Book Description

This is the first book in the field to focus on these aspects, providing extremely valuable information unavailable elsewhere for anyone seeking the practical application of microreactor technology in preparative chemistry. The topics covered branch out in three different directions. To begin with, the knowledge necessary for the preparative chemistry concerning the influence of the so-called microeffects on the reaction procedure and on mass and heat transfer as well as the surface phenomena are provided in detail. Next, practical aspects of the synthesis of various basic chemicals and fine chemicals, polymers, bioproducts and nanoparticles are discussed, including important advice for both the researcher and industrial chemist. Finally, reaction examples in microreactors whose reaction guidance are best understood are given together with universally applicable correlations as well as modeling approaches and transfer potential on related reaction systems. With its specific instructions, tips and experimental procedures for product syntheses as well as the inclusion of both the technical and theoretical background this is a must-have for beginners and experts alike working in this emerging field.



Microreactors in Organic Chemistry and Catalysis

Author : Thomas Wirth

Publisher : John Wiley & Sons

Page : 493 pages

File Size : 26,8 MB

Release : 2013-02-22

Category : Science

ISBN : 3527659749

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Book Description

For the second edition of 'Microreactors in Organic Chemistry and Catalysis' all chapters have been revised and updated to reflect the latest developments in this rapidly developing field. This new edition has 60% more content, and it remains a comprehensive publication covering most aspects of the topic. The use of microreactors in homogeneous, heterogeneous as well as biphasic reactions is covered in the main part of the book, together with catalytic, bioorganic and automation approaches. The initial chapters also provide a solid physical chemistry background on fluidics in microdevices. Finally, a chapter on industrial applications and developments covers recent progress in process chemistry. An excellent reference for beginners and experts alike.



Flow and Microreactor Technology in Medicinal Chemistry

Author : Esther Alza

Publisher : John Wiley & Sons

Page : 372 pages

File Size : 37,32 MB

Release : 2022-06-13

Category : Science

ISBN : 3527824618

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Book Description

Learn to master a powerful technology to enable a faster drug discovery workflow The ultimate dream for medicinal chemists is the ability to synthesize new drug-like compounds with the push of a button. The key to synthesizing chemical compounds more quickly and accurately lies in computer-controlled technologies that can be optimized by machine learning. Recent developments in computer-controlled automated syntheses that rely on miniature flow reactors—with integrated analysis of the resulting products—provide a workable technology for synthesizing new chemical substances very quickly and with minimal effort. In Flow and Microreactor Technology in Medicinal Chemistry, early adopters of this ground-breaking technology describe its current and potential uses in medicinal chemistry. Based on successful examples of the use of flow and microreactor synthesis for drug-like compounds, the book introduces current as well as emerging uses for automated synthesis in a drug discovery context. Flow and Microreactor Technology in Medicinal Chemistry readers will also find: Numerous case studies that address the most common applications of this technology in the day-to-day work of medicinal chemists How to integrate flow synthesis with drug discovery How to perform enantioselective reactions under continuous flow conditions Flow and Microreactor Technology in Medicinal Chemistry is a valuable practical reference for medicinal chemists, organic chemists, and natural products chemists, whether they are working in academia or in the pharmaceutical industry.



Basics of Flow Microreactor Synthesis

Author : Jun-ichi Yoshida

Publisher : Springer

Page : 111 pages

File Size : 50,25 MB

Release : 2015-05-08

Category : Science

ISBN : 4431555137

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Book Description

This book provides in a concise form the principles and applications of flow microreactors in organic and polymer synthesis. Recently, it became possible to conduct chemical reactions in a flow reactor in laboratory synthesis. The flow microreactor enables reactions that cannot be done in batch, opening a new possibility of chemical synthesis. Extremely fast mass and heat transfer and high-resolution residence time control are responsible for the remarkable features of that process. The book is not an exhaustive compilation of all known examples of flow microreactor synthesis. Rather, it is a sampling of sufficient variety to illustrate the concept, the scope, and the current state of flow microreactor synthesis. Researchers both in academia and in industry will be interested in this book because the topics encompassed by the book are vigorously studied in many university and company laboratories today.



Continuous-Flow Chemistry in the Research Laboratory

Author : Toma Glasnov

Publisher : Springer

Page : 119 pages

File Size : 34,19 MB

Release : 2016-06-01

Category : Science

ISBN : 331932196X

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Book Description

This book presents a short introduction to the historical background to the field, the state of the art and a brief survey of the available instrumentation and the processing techniques used. The following major areas of interest in synthetic, organic and medicinal chemistry are elaborated on: transition-metal catalyzed reactions, organocatalytic transformations, heterocyclic synthesis, and photochemical reactions. Finally, selected applications in industry are also discussed. With its ample presentation of examples from recent literature, this is an essential and reliable source of information for both experienced researchers and postgraduate newcomers to the field.



Flash Chemistry

Author : Jun-ichi Yoshida

Publisher : John Wiley & Sons

Page : 244 pages

File Size : 30,31 MB

Release : 2008-10-13

Category : Science

ISBN : 0470723416

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Book Description

Have you ever wished you could speed up your organic syntheses without losing control of the reaction? Flash Chemistry is a new concept which offers an integrated scheme for fast, controlled organic synthesis. It brings together the generation of highly reactive species and their reactions in Microsystems to enable highly controlled organic syntheses on a preparative scale in timescales of a few seconds or less. Flash Chemistry: Fast Organic Synthesis in microsystems is the first book to describe this exciting new technique, with chapters covering: an introduction to flash chemistry reaction dynamics: how fast is the act of chemical transformation, what is the rate of reaction, and what determines the selectivity of a reaction? examples of why flash chemistry is needed: the rapid construction of chemical libraries, rapid synthesis of radioactive PET probes, and on-demand rapid synthesis in industry the generation of highly reactive species through thermal, microwave, chemical, photochemical, and electrochemical activation microsystems: What are microsystems and how are they made? Why is size so important? What are the characteristic features of microsystems? conduction and control of extremely fast reactions using microsystems applications of flash chemistry in organic synthesis polymer synthesis based on flash chemistry industrial applications of flash chemistry Flash Chemistry: Fast Organic Synthesis in Microsystems is an essential introduction to anyone working in organic synthesis, process chemistry, chemical engineering and physical organic chemistry concerned with fundamental aspects of chemical reactions an d synthesis and the production of organic compounds.



Flow Chemistry – Fundamentals

Author : Ferenc Darvas

Publisher : Walter de Gruyter GmbH & Co KG

Page : 448 pages

File Size : 29,15 MB

Release : 2021-10-25

Category : Technology & Engineering

ISBN : 3110693674

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Book Description

The fully up-dated edition of the two-volume work covers both the theoretical foundation as well as the practical aspects. Presenting the complete insight into driving a chemical reaction provides a deep understanding for new potential technologies. Updated overview on devices and new key concepts of experimental procedures. Vol. 2: Applications.



Design and Engineering of Microreactor and Smart-Scaled Flow Processes

Author : Volker Hessel

Publisher : MDPI

Page : 250 pages

File Size : 19,62 MB

Release : 2018-10-08

Category : Technology & Engineering

ISBN : 3038420387

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Book Description

This book is a printed edition of the Special Issue "Design and Engineering of Microreactor and Smart-Scaled Flow Processes" that was published in Processes



Chemical Micro Process Engineering

Author : Volker Hessel

Publisher : John Wiley & Sons

Page : 712 pages

File Size : 47,75 MB

Release : 2006-03-06

Category : Science

ISBN : 3527605371

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Book Description

Micro process engineering is approaching both academia and industry. With the provision of micro devices and systems by commercial suppliers, one main barrier for using these units has been eliminated. More and more they become familiar, thereby being one facet of the upheaval in chemical industry. This book focuses on processes rather than on devices: what is 'before' and 'behind' micro device fabrication. A comprehensive and detailed overview is given on: - A multi-faceted, hierarchic analysis of chemical micro process technology - Modelling and simulation of micro reactors - Liquid- and liquid/liquid-phase reactions - Gas/liquid reactions - Gas-phase reactions (heterogeneous catalysis)



Sustainable Process Engineering

Author : Andrzej Benedykt Koltuniewicz

Publisher : Walter de Gruyter GmbH & Co KG

Page : 433 pages

File Size : 28,86 MB

Release : 2014-08-19

Category : Science

ISBN : 3110373262

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Book Description

The vital need for alternative resources and reaction routes, environmentally friendly and economically feasible industrial chemical processes has become a ubiquitous reality. This very timely introductory text covers new materials, processes and industry sectors: nanotechnology, microreactors, membrane separations, hybrid processes, clean technologies, energy savings and safe production of energy, renewables and biotechnology. Some completely new processes for the solid-liquid systems are also discussed in detail, thus creating new opportunities of sustainable development not only in industrial practice.