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Organic Trace Analysis by Liquid Chromatography

Author : James Lawrence

Publisher : Elsevier

Page : 301 pages

File Size : 26,62 MB

Release : 2012-12-02

Category : Science

ISBN : 0323157025

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Book Description

Organic Trace Analysis by Liquid Chromatography focuses on high-performance liquid chromatography in the field of formulations analysis, which includes quality control of pharmaceutical preparations, pesticide formulations, cosmetics, and food colors. This book explores the application of liquid chromatography to trace analysis. Organized into 10 chapters, this book starts with an overview of the special requirements of liquid chromatography for trace analysis. This text then compares the approach to gas chromatography and formulations analysis, noting the significant difference. Other chapters consider the liquid chromatography equipment and examine the best types and conditions of instrumentation suitable for trace analysis. This book discusses as well the chromatography theory and includes descriptive accounts of the principles of the different forms of chromatography. The final chapter describes the typical approaches that are used for trace analysis. This book is a valuable resource for analysts engaged in the determination of trace organics in many various substrates.



Organic Trace Analysis

Author : Reinhard Nießner

Publisher : Walter de Gruyter GmbH & Co KG

Page : 369 pages

File Size : 41,74 MB

Release : 2017-08-07

Category : Science

ISBN : 3110432935

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Book Description

"Organic Trace Analysis" presents the basics of trace analysis, from sample preparation to the measurement: Students are introduced to statistical evaluation, quality control technologies, sampling and preparation of organic traces, as well as to enrichment and separation of samples. Spectroscopic techniques as chromatography, capillary electrophoresis, mass spectrometry, and receptor-based bioanalysis are presented in detail.



Sample Handling and Trace Analysis of Pollutants

Author : Damia Barcelo

Publisher : Elsevier

Page : 1151 pages

File Size : 26,95 MB

Release : 2000-03-08

Category : Science

ISBN : 0080540694

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Book Description

This book is an updated, completely revised version of a previous volume in this series entitled: ENVIRONMENTAL ANALYSIS -- Techniques, applications and quality assurance. The book treats different aspects of environmental analysis such as sample handling and analytical techniques, the applications to trace analysis of pollutants (mainly organic compounds), and quality assurance aspects, including the use of certified reference materials for the quality control of the whole analytical process. New analytical techniques are presented that have been developed significantly over the last 6 years, like solid phase microextraction, microwave-assisted extraction, liquid chromatography-mass spectrometric methods, immunoassays, and biosensors. The book is divided into four sections. The first describes field sampling techniques and sample preparation in environmental matrices: water, soil, sediment and biota. The second section covers the application areas which are either based on techniques, like the use of gas chromatography-atomic emission detection, immunoassays, or coupled-column liquid chromatography, or on specific application areas, like chlorinated compounds, pesticides, phenols, mycotoxins, phytotoxins, radionuclides, industrial effluents and wastes, including mine waste. Validation and quality assurance are described in the third section, together with the interpretation of environmental data using advanced chemometric techniques. The final section reports the use of somewhat advanced analytical methods, usually more expensive, less routinely used or less developed, for the determination of pollutants.



Organic Trace Analysis

Author : Reinhard Nießner

Publisher : Walter de Gruyter GmbH & Co KG

Page : 370 pages

File Size : 28,10 MB

Release : 2017-08-07

Category : Science

ISBN : 3110441152

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Book Description

"Organic Trace Analysis" presents the basics of trace analysis, from sample preparation to the measurement: Students are introduced to statistical evaluation, quality control technologies, sampling and preparation of organic traces, as well as to enrichment and separation of samples. Spectroscopic techniques as chromatography, capillary electrophoresis, mass spectrometry, and receptor-based bioanalysis are presented in detail.



Organic Trace Analysis

Author : Reinhard Nießner

Publisher : Walter de Gruyter GmbH & Co KG

Page : 682 pages

File Size : 21,75 MB

Release : 2024-09-23

Category : Technology & Engineering

ISBN : 3111166139

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Book Description

Organic contaminants even in very low concentrations can have toxic and ecotoxic effects on exposed organisms. Detection and quantification of such trace amounts in diverging matrices (e.g., water, air, soil, food, tissue, organisms) is challenging and great carefulness and strategic thinking is needed to get reliable results along the way from taking samples up to the final analysis. In the 2nd edition, besides revisions of existing chapters, new analytical technologies and recent application examples are presented: non-target mass spectrometric analysis, trace analysis of per- and polyfluoroalkylated "forever chemicals", organophosphorus esters (nerve agents), and micro- and nanoplastic particles in the environment. Students will learn about peculiarities and state of the art organic trace analysis and acquire basic and advanced principles of statistical evaluation of analytical results quality control strategies and good laboratory practices sampling techniques from various matrices sample treatment, enrichment and clean-up techniques chromatographic analyses including hyphenated techniques, and spectroscopy as well mass spectrometry and bioanalytical tools. An extended chapter on selected applications will transfer the theoretical understanding into applied scientific problems. Students will profit from a comprehensive and state of the art overview of organic trace analyses and from an extensive collection of relevant literature.





Handbook of Trace Analysis

Author : Irena Baranowska

Publisher : Springer

Page : 458 pages

File Size : 15,30 MB

Release : 2015-08-13

Category : Science

ISBN : 3319196146

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Book Description

This handbook is unique in its comprehensive coverage of the subject and focus on practical applications in diverse fields. It includes methods for sample preparation, the role of certified reference materials, calibration methods and statistical evaluation of the results. Problems concerning inorganic and bioinorganic speciation analysis, as well as special aspects such as trace analysis of noble metals, radionuclides and volatile organic compounds are also discussed. A significant part of the content presents applications of methods and procedures in medicine (metabolomics and therapeutic drug monitoring); pharmacy (the analysis of contaminants in drugs); studies of environmental samples; food samples and forensic analytics – essential examples that will also facilitate problem solving in related areas.



Trace Analysis

Author : Peter Bedson

Publisher : Royal Society of Chemistry

Page : 420 pages

File Size : 26,73 MB

Release : 2007-10-31

Category : Science

ISBN : 1847559409

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Book Description

Trace Analysis is a highly practical book which deals with the science rather than the paperwork of quality assurance systems. Produced as part of the UK Valid Analytical Measurement (VAM) initiative, it provides the analyst with a systematic approach across the broad spectrum of trace analysis, offering practical advice and guidance on methodology and techniques. The book is structured to take the analyst step-by-step through the stages of any trace analysis. The approach is general, being broken down only into types of analyte. Additional chapters explain the application of groups of techniques to each analyte type. Each section contains references to published material which will allow the analyst to obtain further information on specific topics. Throughout the book, the analyst is reminded of pitfalls which lead to unreliable results. This new book therefore offers invaluable advice to analysts in all areas and at all levels, providing practical 'expert' advice on methodology. It will prove indispensable as a single, comprehensive bench guide for analysts in university, college and industrial laboratories.



Trace Analysis

Author : James F. Lawrence

Publisher : Elsevier

Page : 318 pages

File Size : 37,91 MB

Release : 2013-10-22

Category : Science

ISBN : 1483264068

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Book Description

Trace Analysis, Volume 4 presents critical discussions of selected topics in organic and inorganic analytical chemistry including instrumentation, techniques, and applications to the detection, identification, and quantitation of trace quantities of substances in a large variety of sample materials. The volume is directed towards topics in the trace analysis of biological materials and environmental samples. Chapters are devoted to discussions on developments and applications of ion-selective polymeric membrane electrodes for biological tissues and fluids; evaluation of X-ray emission spectroscopy for trace analysis; the use of solid adsorbents for pre-concentrating trace organic substances, mainly pollutants, from air; and comparison of neutron activation analysis and proton-induced X-ray emission spectroscopy for the determination of trace elements in rain and snow. Organic and inorganic chemists, medical technicians, and ecologists will find the book a good reference material.



Green Analytical Chemistry

Author : Justyna Płotka-Wasylka

Publisher : Springer

Page : 460 pages

File Size : 44,48 MB

Release : 2019-08-02

Category : Science

ISBN : 981139105X

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Book Description

The book explains the principles and fundamentals of Green Analytical Chemistry (GAC) and highlights the current developments and future potential of the analytical green chemistry-oriented applications of various solutions. The book consists of sixteen chapters, including the history and milestones of GAC; issues related to teaching of green analytical chemistry and greening the university laboratories; evaluation of impact of analytical activities on the environmental and human health, direct techniques of detection, identification and determination of trace constituents; new achievements in the field of extraction of trace analytes from samples characterized by complex composition of the matrix; “green” nature of the derivatization process in analytical chemistry; passive techniques of sampling of analytes; green sorption materials used in analytical procedures; new types of solvents in the field of analytical chemistry. In addition green chromatography and related techniques, fast tests for assessment of the wide spectrum of pollutants in the different types of the medium, remote monitoring of environmental pollutants, qualitative and comparative evaluation, quantitative assessment, and future trends and perspectives are discussed. This book appeals to a wide readership of the academic and industrial researchers. In addition, it can be used in the classroom for undergraduate and graduate Ph.D. students focusing on elaboration of new analytical procedures for organic and inorganic compounds determination in different kinds of samples characterized by complex matrices composition.Jacek Namieśnik was a Professor at the Department of Analytical Chemistry, Gdańsk University of Technology, Poland. Justyna Płotka-Wasylka is a teacher and researcher at the same department.