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Preconcentration Techniques For Trace Elements

Author : Zeev Alfassi

Publisher : CRC Press

Page : 490 pages

File Size : 47,57 MB

Release : 1991-12-07

Category : Science

ISBN : 9780849352133

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Book Description

Accurate determination of trace elements is critical in various fields of science and technology. Direct measurement of trace elements in samples with complex matrices is often impractical, either due to analytical sensitivity limitations or matrix interferences. Preconcentration procedures are generally needed to eliminate matrix interferences and/or enrich minute amounts of analytes to a level for reliable measurements. Preconcentration Techniques for Trace Elements provides up-to-date information on various preconcentration techniques and detailed discussions regarding such topics as the dissolution of matrices, coprecipitation, solvent extraction, electrochemical means, ion exchange, sorption, chromatographic methods, flotation, membranes, volatization, polymer foam sorbents, fire assay, isotachophoresis, and filter papers. This comprehensive volume, featuring contributions from 21 experts from nine countries, will provide valuable reference material for all scientists and technicians dealing with trace analysis of real-world samples.



Determination of Trace Elements

Author : Zeev B. Alfassi

Publisher : Wiley-VCH

Page : 632 pages

File Size : 23,87 MB

Release : 1994-10-17

Category : Science

ISBN :

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Book Description

Determination of Trace Elements Edited by Zeev B. Alfassi The best way to determine trace elements! This easy-to-use handbook guides the reader through the maze of all modern analytical operations. Each method is described by an expert in the field. The book highlights the advantages and disadvantages of individual techniques and enables pharmacologists, environmentalists, material scientists, and food industry to select a judicious procedure for their trace element analysis.



Sample Preparation for Trace Element Analysis

Author : Zoltan Mester

Publisher : Elsevier

Page : 1339 pages

File Size : 12,28 MB

Release : 2003-12-16

Category : Science

ISBN : 0080545483

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Book Description

Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation.- First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.



Vapor Generation Techniques for Trace Element Analysis

Author : Alessandro D'Ulivo

Publisher : Elsevier

Page : 476 pages

File Size : 23,97 MB

Release : 2022-04-25

Category : Science

ISBN : 0323858341

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Book Description

Vapor Generation Techniques for Trace Element Analysis: Fundamental Aspects provides an overview and discussion of the fundamental aspects governing derivatization reactions of trace-level elements for analytical purposes. Vapor generation techniques coupled with atomic or mass spectrometry have been employed for over 50 years, but their popularity has dramatically increased in recent years, especially as alternative vapor generation approaches have been developed. This book bridges the knowledge gap of the derivatization mechanisms that yield volatile compounds and provides an update on recent developments in vapor generation techniques used for the determination and speciation of trace elements by atomic optical and mass spectrometry. It will serve as a comprehensive, single-source overview of recent developments, providing readers with an understanding of the correct implementation-and limitations-of applying vapor generation techniques to everyday analytical problems facing the trace element analyst. Covers reaction mechanisms and fundamental processes of vapor generation in detail Includes classical and alternative vapor generation approaches: alkylation, chelation, plasma, photochemical and electrochemical Guides the interpretation of experimental results and implementation of vapor generation techniques in the laboratory



A Handbook of Silicate Rock Analysis

Author : P.J. Potts

Publisher : Springer Science & Business Media

Page : 633 pages

File Size : 24,45 MB

Release : 2013-11-11

Category : Science

ISBN : 940153988X

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Book Description

without an appreciation of what happens in between. The techniques available for the chemical analysis of silicate rocks have undergone a revolution over the last 30 years. However, to use an analytical technique most effectively, No longer is the analytical balance the only instrument used it is essential to understand its analytical characteristics, in for quantitative measurement, as it was in the days of classi particular the excitation mechanism and the response of the cal gravimetric procedures. A wide variety of instrumental signal detection system. In this book, these characteristics techniques is now commonly used for silicate rock analysis, have been described within a framework of practical ana lytical aplications, especially for the routine multi-element including some that incorporate excitation sources and detec tion systems that have been developed only in the last few analysis of silicate rocks. All analytical techniques available years. These instrumental developments now permit a wide for routine silicate rock analysis are discussed, including range of trace elements to be determined on a routine basis. some more specialized procedures. Sufficient detail is In parallel with these exciting advances, users have tended included to provide practitioners of geochemistry with a firm to become more remote from the data production process. base from which to assess current performance, and in some This is, in part, an inevitable result of the widespread intro cases, future developments.



Modern Methods for Trace Element Determination

Author : C. Vandecasteele

Publisher : John Wiley & Sons

Page : 352 pages

File Size : 50,12 MB

Release : 1997-03-06

Category : Science

ISBN : 9780471974451

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Book Description

Spurenanalyse von den theoretischen Grundlagen über die apparative Ausrüstung bis zur Probenpräparation - dieses Buch bringt Ihr Wissen über ICP-MS, HPLC-AAS, HPLC-ICP-MS und konventionellere Methoden auf den aktuellsten Stand. Viele Illustrationen und Beispiele aus der Praxis - so der biologischen Analytik und der Analytik hochreiner Materialien - empfehlen das Buch besonders für fortgeschrittene Studenten und Graduierte.



Handbook of Trace Analysis

Author : Irena Baranowska

Publisher : Springer

Page : 458 pages

File Size : 23,33 MB

Release : 2015-08-13

Category : Science

ISBN : 3319196146

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Book Description

This handbook is unique in its comprehensive coverage of the subject and focus on practical applications in diverse fields. It includes methods for sample preparation, the role of certified reference materials, calibration methods and statistical evaluation of the results. Problems concerning inorganic and bioinorganic speciation analysis, as well as special aspects such as trace analysis of noble metals, radionuclides and volatile organic compounds are also discussed. A significant part of the content presents applications of methods and procedures in medicine (metabolomics and therapeutic drug monitoring); pharmacy (the analysis of contaminants in drugs); studies of environmental samples; food samples and forensic analytics – essential examples that will also facilitate problem solving in related areas.



Trace Analysis

Author : Peter Bedson

Publisher : Royal Society of Chemistry

Page : 420 pages

File Size : 37,5 MB

Release : 2007-10-31

Category : Science

ISBN : 1847559409

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Book Description

Trace Analysis is a highly practical book which deals with the science rather than the paperwork of quality assurance systems. Produced as part of the UK Valid Analytical Measurement (VAM) initiative, it provides the analyst with a systematic approach across the broad spectrum of trace analysis, offering practical advice and guidance on methodology and techniques. The book is structured to take the analyst step-by-step through the stages of any trace analysis. The approach is general, being broken down only into types of analyte. Additional chapters explain the application of groups of techniques to each analyte type. Each section contains references to published material which will allow the analyst to obtain further information on specific topics. Throughout the book, the analyst is reminded of pitfalls which lead to unreliable results. This new book therefore offers invaluable advice to analysts in all areas and at all levels, providing practical 'expert' advice on methodology. It will prove indispensable as a single, comprehensive bench guide for analysts in university, college and industrial laboratories.



Separation, Preconcentration and Spectrophotometry in Inorganic Analysis

Author : Z. Marczenko

Publisher : Elsevier

Page : 526 pages

File Size : 11,62 MB

Release : 2000-10-18

Category : Science

ISBN : 0080541089

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Book Description

Spectrophotometry enables one to determine, with good precision and sensitivity, almost all the elements present in small and trace quantities of any material. The method is particularly useful in the determination of non-metals and allows the determination elements in a large range of concentrations (from single % to low ppm levels) in various materials.In Separation, Preconcentration and Spectrophotometry in Inorganic Analysis, much attention has been paid to separation and preconcentration methods, since they play an essential role in increasing the selectivity and sensitivity of spectrophotometric methods. Separation and preconcentration methods have also been utilised in other determination techniques.Spectrophotometric methods which are widely used for the determination of the elements in a large variety of inorganic materials are presented in the book whilst separation and preconcentration procedures combined with spectrophotometry are also described. This book contains recent advances in spectrophotometry, detailed discussion of the instrumentation, and the techniques and reagents used for spectrophotometric determination of elements in a wide range of materials as well as a detailed discussion of separation and preconcentration procedures that precede the spectrophotometric detection.



Preconcentration Techniques for Natural and Treated Waters

Author : T.R. Crompton

Publisher : CRC Press

Page : 740 pages

File Size : 31,5 MB

Release : 2002-10-31

Category : Science

ISBN : 9780415268110

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Book Description

Equipment used for the analysis of water is frequently insufficiently sensitive to be able to detect the low concentrations of organic and inorganic substances present in samples. Applying preconcentration to the sample prior to analysis means the results gained are more accurate and can be used to report trends more effectively. Each chapter of Preconcentration Techniques for Natural and Treated Waters discusses a different method of preconcentration and its application to the preconcentration of cations, anions, organic substances and organometallic compounds. Drawing together the recent world literature available on the subject, this book provides detailed discussion of the need for reducing detection limits in analytical chemistry and ways of achieving this aim. Throughout the book emphasis is laid on providing practical experimental detail, facilitating further development of procedures. Numerous tables present information clearly and accessibly. This book will be an invaluable reference for biologists, chemists, agriculturists, toxicologists, oceanographers, and environmentalists dealing with the analysis of water in industry and academia.