Author : L. Ebdon
Publisher : John Wiley & Sons
Page : 212 pages
File Size : 42,96 MB
Release : 1998-04-08
Category : Science
ISBN : 9780471974185
Das umfassende Handbuch der Atomspektroskopie jetzt in sorgfältig überarbeiteter, noch besser organisierter zweiter Auflage! Ergänzt wurden Kapitel zu wichtigen neuen Verfahren wie der Plasma-Atomemissionsspektroskopie und der ICP-Massenspektrometrie. Fettgedruckte Stichworte, übersichtliche Diagramme und praktische Übungen erleichtern das Erarbeiten und Vertiefen des Stoffes. (02/98)
Author : J. Sneddon
Publisher : Elsevier
Page : 396 pages
File Size : 41,89 MB
Release : 2012-12-02
Category : Science
ISBN : 044459910X
A comprehensive and detailed description of the most widely used sample introduction techniques in atomic spectroscopy is presented in this volume. Comprising twelve separate chapters, the book describes the theory in detail, and gives an account of techniques and selected applications of sample introduction systems. The first chapter is a general overview on sample introduction. The remaining eleven chapters are each devoted to a specific sample introduction and deal with the basic principles, describe the system, advantages, disadvantages and selected applications. Systems described are: pneumatic nebulization, electrothermal vaporization, laser ablation, impaction/electrostatic precipitation, slurry atomization, ultrasonic and thermospray nebulization, hydride generation, chromatographic, spark and arc, low-pressure discharges, flow injection analysis and direct solid introduction. Each chapter is suitable for a separate discussion. Being a unique textbook in this field, Sample Introduction in Atomic Spectroscopy should prove invaluable for courses at graduate level.
Author : L Lajunen
Publisher : Royal Society of Chemistry
Page : 355 pages
File Size : 29,86 MB
Release : 2007-10-31
Category : Science
ISBN : 1847551904
This book describes both the theory of atomic spectroscopy and all the major atomic spectrometric techniques (AAS, Flame-AES, Plasma AES, AFS, and ICP-MS), including basic concepts, instrumentation and applications. Spectrochemical Analysis by Atomic Absorption and Emission is very wide in scope and will be extremely useful to both undergraduates and lecturers undertaking modern analytical chemistry courses. It contains many figures and tables which illuminate the text, covers various sample preparation methods and gives suggestions for further reading.
Author : Maaz Khan
Publisher : BoD – Books on Demand
Page : 144 pages
File Size : 16,36 MB
Release : 2020-03-04
Category : Science
ISBN : 1789852056
Modern spectroscopic techniques have a number of applications in many fields including material science, physics, chemistry, biology, and medicine. This book, "Modern Spectroscopic Techniques and Applications", presents knowledge about these techniques and their applications. The chapters cover many aspects such as an introduction to atomic microscopy, Raman spectroscopy, infrared spectroscopy and their applications covering both the experimental and theoretical aspects. This book is aimed to provide understanding about modern spectroscopic techniques and their applications to students, scientists, and engineers working in the relevant areas.
Author : Jon Clement Van Loon
Publisher : Academic Press
Page : 360 pages
File Size : 39,18 MB
Release : 1980-03-28
Category : Science
ISBN :
Analysis of water. Analysis of geological materials. Analysis of organic samples. Analysis of metals and alloys. Analysis of air samples. Analysis of petroleum and petroleum products. Analysis of industrial samples. Determination of metal compounds. Expected new developments in atomic spectroscopy.
Author : Jose Andrade-Garda
Publisher : Royal Society of Chemistry
Page : 431 pages
File Size : 37,71 MB
Release : 2015-11-09
Category : Science
ISBN : 1782625445
The first edition of this book was a first book for atomic spectroscopists to present the basic principles of experimental designs, optimization and multivariate regression. Multivariate regression is a valuable statistical method for handling complex problems (such as spectral and chemical interferences) which arise during atomic spectrometry. However, the technique is underused as most spectroscopists do not have time to study the often complex literature on the subject. This practical introduction uses conceptual explanations and worked examples to give readers a clear understanding of the technique. Mathematics is kept to a minimum but, when required, is kept at a basic level. Practical considerations, interpretations and troubleshooting are emphasized and literature surveys are included to guide the reader to further work. The same dataset is used for all chapters dealing with calibration to demonstrate the differences between the different methodologies. Readers will learn how to handle spectral and chemical interferences in atomic spectrometry in a new, more efficient and cost-effective way.
Author : Muhammad Sajid Hamid Akash
Publisher : Springer Nature
Page : 235 pages
File Size : 30,81 MB
Release : 2019-12-17
Category : Medical
ISBN : 9811515476
Recent advances in the pharmaceutical sciences and biotechnology have facilitated the production, design, formulation and use of various types of pharmaceuticals and biopharmaceuticals. This book provides detailed information on the background, basic principles, and components of techniques used for the analysis of pharmaceuticals and biopharmaceuticals. Focusing on those analytical techniques that are most frequently used for pharmaceuticals, it classifies them into three major sections and 19 chapters, each of which discusses a respective technique in detail. Chiefly intended for graduate students in the pharmaceutical sciences, the book will familiarize them with the components, working principles and practical applications of these indispensable analytical techniques.
Author : Bernhard Welz
Publisher : John Wiley & Sons
Page : 296 pages
File Size : 19,23 MB
Release : 2006-03-06
Category : Science
ISBN : 3527606378
High-resolution continuum source atomic absorption spectrometry (HR-CS AAS) is the most revolutionary innovation since the introduction of AAS in 1955. Here, the authors provide the first complete and comprehensive discussion of HR-CS AAS and its application to the analysis of a variety of difficult matrices. Published just in time with the first commercial instrument available for this new technique, the book is a must for all those who want to know more about HR-CS AAS, and in particular for all future users. The advantages of the new technique over conventional line-source AAS are clearly demonstrated using practical examples and numerous figures, many in full color. HR-CS AAS is overcoming essentially all the remaining limitations of established AAS, particularly the notorious problem of accurate background measurement and correction. Using a continuum radiation source and a CCD array detector makes the spectral environment visible to several tenths of a nanometer on both sides of the analytical line, tremendously facilitating method development and elimination of interferences. Conceived as a supplement to the standard reference work on AAS by B. Welz and M. Sperling, this book does not repeat such fundamentals as the principles of atomizers or atomization mechanisms. Instead, it is strictly focused on new and additional information required to profit from HR-CS AAS. It presents characteristic concentration for flame atomization and characteristic mass data for electrothermal atomization for all elements, as well as listing numerous secondary lines of lower sensitivity for the determination of higher analyte concentrations. The highly resolved molecular absorption spectra of nitric, sulfuric and phosphoric acids, observed in an air-acetylene flame, which are depicted together with the atomic lines of all elements, make it possible to predict potential spectral interferences.
Author : Robert Thomas
Publisher : CRC Press
Page : 474 pages
File Size : 43,72 MB
Release : 2018-01-29
Category : Medical
ISBN : 1351984403
Recent regulations on heavy metal testing have required the pharmaceutical industry to monitor a suite of elemental impurities in pharmaceutical raw materials, drug products and dietary supplements. These new directives s are described in the new United States Pharmacopeia (USP) Chapters , , and , together with Q3D, Step 4 guidelines for elemental impurities, drafted by the ICH (International Conference on Harmonization of Technical Requirements for Registration of Pharmaceuticals for Human Use), a consortium of global pharmaceutical associations, including the European Pharmacopeia (Ph.Eur.), the Japanese Pharmacopeia (JP) and the USP. This book provides a complete guide to the analytical methodology, instrumental techniques and sample preparation procedures used for measuring elemental impurities in pharmaceutical and nutraceutical materials. It offers readers the tools to better understand plasma spectrochemistry to optimize detection capability for the full suite of elemental PDE (Permitted Daily Exposure) levels in the various drug delivery categories. Other relevant information covered in the book includes: The complete guide to measuring elemental impurities in pharmaceutical and nutraceutical materials. Covers heavy metals testing in the pharmaceutical industry from an historical perspective. Gives an overview of current USP Chapters and and ICH Q3D Step 4 Guidelines. Explains the purpose of validation protocols used in Chapter , including how J-values are calculated Describes fundamental principles and practical capabilities of ICP-MS and ICP-OES. Offers guidelines about the optimum strategy for risk assessment Provides tips on how best to prepare and present your data for regulatory inspection. An indispensable resource, the fundamental principles and practical benefits of ICP-OES and ICP-MS are covered in a reader-friendly format that a novice, who is carrying out elemental impurities testing in the pharmaceutical and nutraceutical communities, will find easy to understand.
Author : Ernest Angino
Publisher : Elsevier
Page : 202 pages
File Size : 50,53 MB
Release : 2012-12-02
Category : Science
ISBN : 0444601880
Atomic Absorption Spectrometry in Geology, Second Edition, aims to introduce geologists to the basic simplicity and applicability of atomic absorption spectrometry as it relates to geologic problems; to provide a summary of applications of atomic absorption to geology that are at scattered throughout the literature; and to encourage the accelerated application of atomic absorption spectrometry to geological problems. The book is organized into two parts. The first part, ""Theory and instrumentation,"" explains the theory of atomic absorption spectrophotometry; the operation of the atomic absorption spectrophotometer; and the types of interferences in atomic absorption spectrometry. The second part, ""Methods and applications,"" deals with applications of the atomic absorption method, including detection of the metal content of natural waters; metallic content of ores; and the analysis of trace elements in rocks and minerals. Also discussed are applications of the atomic absorption method in marine geochemistry and for isotopic abundance studies. The book includes some Appendices to the First Edition.
