Flow Injection Analysis: Instrumentation And Applications


Book Description

The concept of flow injection analysis (FIA) was introduced in the mid-seventies. It was preceded by the success of segmented flow analysis, mainly in clinical and environmental analysis. This advance, as well as the development of continuous monitors for process control and environmental monitors, ensured the success of the FIA methodology. As an exceptionally effective means of mechanization for various procedures of wet chemical analysis, the FIA methodology, in use with a whole arsenal of detection methods of modern analytical chemistry, proved to be of great interest to many.The fast and intensive development of the FIA methodology was due to several factors essential for routine analytical determinations, such as very limited sample consumption, the short analysis time based on a transient signal measurement in a flow-through detector and an on-line carrying out difficult operations of separation, preconcentration or physicochemical conversion of analytes into detectable species.Twenty-year studies by numerous research groups all over the world have provided significant progress in the theoretical description of dispersion phenomena in FIA and various operations of physicochemical treatment of the analyte. This volume is devoted to the presentation of the current status of development of the instrumentation for FIA and the many fields of its practical applications, based on an extensive bibliography of original research publications.




Flow Injection Analysis


Book Description

Annotation The first five chapters in this manual for users and manufacturers of FIA technology describe the principles and properties of detection methods, including molecular and atomic spectroscopy detection methods, electrochemical methods, enzymatic methods and immunoassays, and photoacoustic spectroscopic detection. Chapters six and seven cover on-line sample processing and speciation analysis. Chapter eight (the longest chapter) discusses applications of flow injection methods in routine analysis, including environmental applications and analysis of food products and biological and mineral materials, clinical analysis, pharmaceutical and biotechnology applications, and process analysis. The last three chapters cover sequential and batch injection techniques, review commercially available instrumentation, and discuss current trends in developments of flow analysis. Annotation copyrighted by Book News, Inc., Portland, OR.




Flow-injection Analysis


Book Description




Flow Injection Analysis


Book Description

This Second edition of the flow injection analysis (FIA) text which has become a standard in the field in four languages, is written by two pioneers in the field, who have themselves discovered many of the techniques and designed much of the equipment employed in FIA. Newly revised to account for the many recent developments in FIA, this book presents the state-of-the-art in FIA theory, techniques, and future trends. Specific topics covered include continous-flow analyzers, chemical kinetics in an FIA system, theory of dispersion related to FIA, single-line FIA manifolds, FIA determinations based on separation processes, commercially available flow-injection analyzers, the FIA laboratory--a microconduit-based pedagogical system, review of the flow-injection literature, and flow injection analysis now and in the future.




Flow Analysis


Book Description

Flow Analysis: A Practical Guide reviews flow techniques for automating chemical analysis with the goal of increasing efficiency and producing better analytical results. Various applications for flow techniques are reviewed including industrial process monitoring (for example, foods and beverages, drugs and pharmaceuticals); as well as agricultural, life science, radioactivity, and environmental analysis with an emphasis on the latter. This book is a valuable resource for young scientists or graduate-level students who want to learn how to introduce flow techniques into their experiments, and for experts who need specific and technical details to develop complete experimental systems. - Includes descriptions of the theoretical and technical bases of the most important flow techniques - Focuses on new trends in the field such as using flow techniques for radioactivity and environmental applications - Features instructions for coupling different types of detectors online with flow systems




Green Analytical Chemistry


Book Description

The book explains the principles and fundamentals of Green Analytical Chemistry (GAC) and highlights the current developments and future potential of the analytical green chemistry-oriented applications of various solutions. The book consists of sixteen chapters, including the history and milestones of GAC; issues related to teaching of green analytical chemistry and greening the university laboratories; evaluation of impact of analytical activities on the environmental and human health, direct techniques of detection, identification and determination of trace constituents; new achievements in the field of extraction of trace analytes from samples characterized by complex composition of the matrix; “green” nature of the derivatization process in analytical chemistry; passive techniques of sampling of analytes; green sorption materials used in analytical procedures; new types of solvents in the field of analytical chemistry. In addition green chromatography and related techniques, fast tests for assessment of the wide spectrum of pollutants in the different types of the medium, remote monitoring of environmental pollutants, qualitative and comparative evaluation, quantitative assessment, and future trends and perspectives are discussed. This book appeals to a wide readership of the academic and industrial researchers. In addition, it can be used in the classroom for undergraduate and graduate Ph.D. students focusing on elaboration of new analytical procedures for organic and inorganic compounds determination in different kinds of samples characterized by complex matrices composition.Jacek Namieśnik was a Professor at the Department of Analytical Chemistry, Gdańsk University of Technology, Poland. Justyna Płotka-Wasylka is a teacher and researcher at the same department.




Flow Analysis with Spectrophotometric and Luminometric Detection


Book Description

Machine generated contents note: 1. Introduction 2. Historical view 3. Fundamentals 4. Interaction of radiation with the flowing sample 5. Flow analysers 6. Instrumentation 7. Special strategies for flow manipulation 8. Sample handling.




Electrochemical Sensors, Biosensors and their Biomedical Applications


Book Description

This book broadly reviews the modem techniques and significant applications of chemical sensors and biosensors. Chapters are written by experts in the field – including Professor Joseph Wang, the most cited scientist in the world and renowned expert on sensor science who is also co-editor. Each chapter provides technical details beyond the level found in typical journal articles, and explores the application of chemical sensors and biosensors to a significant problem in biomedical science, also providing a prospectus for the future.This book compiles the expert knowledge of many specialists in the construction and use of chemical sensors and biosensors including nitric oxide sensors, glucose sensors, DNA sensors, hydrogen sulfide sensors, oxygen sensors, superoxide sensors, immuno sensors, lab on chip, implatable microsensors, et al. Emphasis is laid on practical problems, ranging from chemical application to biomedical monitoring and from in vitro to in vivo, from single cell to animal to human measurement. This provides the unique opportunity of exchanging and combining the expertise of otherwise apparently unrelated disciplines of chemistry, biological engineering, and electronic engineering, medical, physiological. - Provides user-oriented guidelines for the proper choice and application of new chemical sensors and biosensors - Details new methodological advancements related to and correlated with the measurement of interested species in biomedical samples - Contains many case studies to illustrate the range of application and importance of the chemical sensors and biosensors




Comprehensive Sampling and Sample Preparation


Book Description

Comprehensive Sampling and Sample Preparation is a complete treatment of the theory and methodology of sampling in all physical phases and the theory of sample preparation for all major extraction techniques. It is the perfect starting point for researchers and students to design and implement their experiments and support those experiments with quality-reviewed background information. In its four volumes, fundamentals of sampling and sample preparation are reinforced through broad and detailed sections dealing with Biological and Medical, Environmental and Forensic, and Food and Beverage applications. The contributions are organized to reflect the way in which analytical chemists approach a problem. It is intended for a broad audience of analytical chemists, both educators and practitioners of the art and can assist in the preparation of courses as well in the selection of sampling and sample preparation techniques to address the challenges at hand. Above all, it is designed to be helpful in learning more about these topics, as well as to encourage an interest in sampling and sample preparation by outlining the present practice of the technology and by indicating research opportunities. Sampling and Sample preparation is a large and well-defined field in Analytical Chemistry, relevant for many application areas such as medicine, environmental science, biochemistry, pharmacology, geology, and food science. This work covers all these aspects and will be extremely useful to researchers and students, who can use it as a starting point to design and implement their experiments and for quality-reviewed background information There are limited resources that Educators can use to effectively teach the fundamental aspects of modern sample preparation technology. Comprehensive Sampling and Sample Preparation addresses this need, but focuses on the common principles of new developments in extraction technologies rather than the differences between techniques thus facilitating a more thorough understanding Provides a complete overview of the field. Not only will help to save time, it will also help to make correct assessments and avoid costly mistakes in sampling in the process Sample and sample preparation are integral parts of the analytical process but are often less considered and sometimes even completely disregarded in the available literature. To fill this gap, leading scientists have contributed 130 chapters, organized in 4 volumes, covering all modern aspects of sampling and liquid, solid phase and membrane extractions, as well as the challenges associated with different types of matrices in relevant application areas




Liquid-Phase Extraction


Book Description

Liquid Phase Extraction thoroughly presents both existing and new techniques in liquid phase extraction. It not only provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample, but also showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including countercurrent chromatography, pressurized-liquid extraction, single-drop Microextraction, and more. Written by recognized experts in their respective fields, it serves as a one-stop reference for those who need to know which technique to choose for liquid phase extraction. Used in conjunction with a similar release, Solid Phase Extraction, it allows users to master this crucial aspect of sample preparation. - Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice - Includes extensive referencing that facilitates the identification of key information - Aimed at both entry-level scientists and those who want to explore new techniques and methods