Techniques in Organic Chemistry


Book Description

Is the most comprehensive and detailed presentation of lab techniques available for organic chemistry students - and the least expensive. It combines specific instructions for 3 different kinds kinds of laboratory glassware and offers extensive coverage of spectroscopic techniques and a strong emphasis on safety issues.




Basic Techniques of Preparative Organic Chemistry


Book Description

Basic Techniques of Preparative Organic Chemistry covers a detailed guide for carrying out the procedures commonly needed in preparative organic chemistry. The book discusses the nature of organic reactions; the basic principles of preparative organic chemistry; unit operations; and good laboratory practice. The text then provides a review of apparatus and equipment and describes the potential hazards involved in a chemical operation, such as toxicity, bodily injuries, smoking, fire, explosion, and implosion. Techniques and unit operations for carrying out a reaction and for isolating and purifying a reaction product; and the criteria for and methods of assessing purity are also considered. The book further tackles packing and storing products and samples and making reports and communications. Students taking organic chemistry courses will find the text useful.




Purification of Laboratory Chemicals


Book Description

Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.* Complete update of this valuable, well-known reference* Provides purification procedures of commercially available chemicals and biochemicals* Includes an extremely useful compilation of ionisation constants




Techniques in Organic Chemistry


Book Description

"Compatible with standard taper miniscale, 14/10 standard taper microscale, Williamson microscale. Supports guided inquiry"--Cover.










The Organic Chem Lab Survival Manual


Book Description

Teaches students the basic techniques and equipment of the organic chemistry lab — the updated new edition of the popular hands-on guide. The Organic Chem Lab Survival Manual helps students understand the basic techniques, essential safety protocols, and the standard instrumentation necessary for success in the laboratory. Author James W. Zubrick has been assisting students navigate organic chemistry labs for more than three decades, explaining how to set up the laboratory, make accurate measurements, and perform safe and meaningful experiments. This practical guide covers every essential area of lab knowledge, from keeping detailed notes and interpreting handbooks to using equipment for chromatography and infrared spectroscopy. Now in its eleventh edition, this guide has been thoroughly updated to cover current laboratory practices, instruments, and techniques. Focusing primarily on macroscale equipment and experiments, chapters cover microscale jointware, drying agents, recrystallization, distillation, nuclear magnetic resonance, and much more. This popular textbook: Familiarizes students with common lab instruments Provides guidance on basic lab skills and procedures Includes easy-to-follow diagrams and illustrations of lab experiments Features practical exercises and activities at the end of each chapter Provides real-world examples of lab notes and instrument manuals The Organic Chem Lab Survival Manual: A Student’s Guide to Techniques, 11th Edition is an essential resource for students new to the laboratory environment, as well as those more experienced seeking to refresh their knowledge.




Techniques and Experiments For Organic Chemistry


Book Description

Embraced by the inside covers' periodic table of elements and table of solutions of acids, the new edition of this introductory text continues to describe laboratory operations in its first part, and experiments in the second. Revisions by Ault (Cornell U.) include detailed instructions for the disposal of waste, and experiments with more interesting compounds (e.g. seven reactions of vanillin, and isolating ibuprofin from ibuprofin tablets). Conscious of costs, microscale experiments are included but not to the point where minuscule amounts of material will preclude the aesthetic pleasure of watching crystals form or distillates collect. Annotation copyrighted by Book News, Inc., Portland, OR




Laboratory Techniques in Organic Chemistry


Book Description

This book deals with general information about work in Organic Chemistry Laboratory, viz., safety, first aid, different types of apparatus and their assemblies used for various types of reactions, stirring arrangements, heating techniques and low temperature experiments. Various methods used for purification of organic compounds have been described. Besides the normal technique, the book includes write-up about molecular distillation, chromatography and electrophoresis. Special emphasis has been given to the methods, which can be used for working up of organic reactions. Various methods, which can be used successfully for isolation of products from natural sources, have been incorporated. Emphasis has also been given on the isolation of products from oily mixture using the technique of Liquid-Liquid extraction. Methods for determining the criteria of purity of organic compounds have been discussed. The book also deals with drying and purification of solvents, preparation of spectroscopical grade solvents and HPCL solvents. The preparation of commonly used deuterated solvents (which are used for NMR spectroscopy work) is a special feature of this book.




Special Distillation Processes


Book Description

Special Distillation Processes, Second Edition focuses on the latest developments in the field, such as separation methods that may prove useful for solving problems encountered during research. Topics include extraction, membrane and adsorption distillation involving the separation principle, process design and experimental techniques. The relationship between processes and techniques are also presented. Comprehensive and easy-to-read, this book provides key information needed to understand processes. It will be a valuable reference source for chemical engineers and students wishing to branch out in chemical engineering. - Provides the only comprehensive book available on special distillation processes - Contains a thorough introduction to recent developments in the field - Presents a valuable reference for students, academics and engineers in chemical engineering