Techniques and Experiments for Advanced Organic Laboratory


Book Description

This book introduces chemists to a variety of techniques which are used in the organic laboratory, including key instrumental analyses such as NMR, capillary GC and GC-MS. Several of the methods, particularly capillary GC and NMR, illustrate the power of modern instrumentation.




Techniques in Organic Chemistry


Book Description

"Compatible with standard taper miniscale, 14/10 standard taper microscale, Williamson microscale. Supports guided inquiry"--Cover.




Comprehensive Organic Chemistry Experiments for the Laboratory Classroom


Book Description

This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment. Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students.







Advanced Organic Synthesis


Book Description

Advanced Organic Synthesis: Methods and Techniques presents a survey and systematic introduction to the modern techniques of organic synthesis. The book attempts to acquaint the reader with a variety of laboratory techniques as well as introduce chemical reagents that require deftness and care in handling. Chapters are devoted that discuss the techniques of organic synthesis; apparatus and terminology used in the description of synthetic procedures; the scope and mechanism of chemical reactions; and technical procedures on how to perform chemical experiments. The text will be of vital importance to advanced undergraduate student or beginning graduate student of chemistry.




Advanced Practical Organic Chemistry, Second Edition


Book Description

The first edition of this book achieved considerable success due to its ease of use and practical approach, and to the clear writing style of the authors. The preparation of organic compounds is still central to many disciplines, from the most applied to the highly academic and, more tan ever is not limited to chemists. With an emphasis on the most up-to-date techniques commonly used in organic syntheses, this book draws on the extensive experience of the authors and their association with some of the world's mleading laboratories of synthetic organic chemistry. In this new edition, all the figures have been re-drawn to bring them up to the highest possible standard, and the text has been revised to bring it up to date. Written primarily for postgraduate, advanced undergraduate and industrial organic chemists, particularly those involved in pharmaceutical, agrochemical and other areas of fine chemical research, the book is also a source of reference for biochemists, biologists, genetic engineers, material scientists and polymer researchers.




High-resolution NMR Techniques in Organic Chemistry


Book Description

From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.




The Organic Chem Lab Survival Manual


Book Description

Teaches students the basic techniques and equipment of the organic chemistry lab — the updated new edition of the popular hands-on guide. The Organic Chem Lab Survival Manual helps students understand the basic techniques, essential safety protocols, and the standard instrumentation necessary for success in the laboratory. Author James W. Zubrick has been assisting students navigate organic chemistry labs for more than three decades, explaining how to set up the laboratory, make accurate measurements, and perform safe and meaningful experiments. This practical guide covers every essential area of lab knowledge, from keeping detailed notes and interpreting handbooks to using equipment for chromatography and infrared spectroscopy. Now in its eleventh edition, this guide has been thoroughly updated to cover current laboratory practices, instruments, and techniques. Focusing primarily on macroscale equipment and experiments, chapters cover microscale jointware, drying agents, recrystallization, distillation, nuclear magnetic resonance, and much more. This popular textbook: Familiarizes students with common lab instruments Provides guidance on basic lab skills and procedures Includes easy-to-follow diagrams and illustrations of lab experiments Features practical exercises and activities at the end of each chapter Provides real-world examples of lab notes and instrument manuals The Organic Chem Lab Survival Manual: A Student’s Guide to Techniques, 11th Edition is an essential resource for students new to the laboratory environment, as well as those more experienced seeking to refresh their knowledge.




Microscale Organic Laboratory


Book Description

This updated revision offers total coverage of organic laboratory experiments and techniques focusing on modern laboratory instrumentation, a strong emphasis on lab safety, additional concentration on sequential reaction sequences, excellent pre- and post-lab exercises, and multistep experiments which maximize the number of manipulations students perform per lab period. The microscale approach is low in cost, offers ease of doing experiments and uses minimal amounts of chemicals. A number of experiments include instructions for scaling up.