Thermal Analysis V1


Book Description

Thermal Analysis, Volume 1: Instrumentation, Organic Materials, and Polymers is a collection of papers presented at the Second International Conference on Thermal Analysis, held in Holy Cross College, Worcester, Massachusetts on August 18-23, 1968. The papers highlight a wide range of applications, from fundamental thermodynamics and kinetics to industrial process development. This book is divided into two major sections encompassing 45 chapters. The first section emphasizes the developments in the instrumentation aspects of thermal analysis. This section deals first with the developments of thermal analysis equipment, methods, and their corresponding application to various fields, including in pharmaceutical research. This section also examines the technique of differential thermal analysis, microcalorimetry, thermogravimetry, mass spectrometry, pyrolysis-flame detection, and thermal volatilization analysis. The second section explores the application of thermal analysis to organic materials, such as polymers and elastomer systems. This section specifically looks into the potential of differential thermal analysis, thermogravimetry, and time-of-flight mass spectrometry in analysis of specific organic materials. Measurements of electrical conductivity, magnetic, dielectric, photoelectric, thermodynamic, and thermophysical properties are also provided.




Thermal Analysis


Book Description

Thermal Analysis deals with the theories of thermal analysis (thermodynamics, irreversible thermodynamics, and kinetics) as well as instrumentation and techniques (thermometry, differential thermal analysis, calorimetry, thermomechanical analysis and dilatometry, and thermogravimetry). Applications of thermal analysis are also described. This book consists of seven chapters and begins with a brief outline of the history and meaning of heat and temperature before listing the techniques of thermal analysis. The reader is then introduced to the basis of thermal analysis, paying particular attention to the macroscopic theories of matter, namely, equilibrium thermodynamics, irreversible thermodynamics, and kinetics. The next chapter discusses thermometry, focusing on the international temperature scale and the techniques of measuring temperature. Examples of heating and cooling curves are linked to the discussion of transitions. The groundwork for a detailed understanding of transition temperature is given. The chapters that follow explore the principles of differential thermal analysis, calorimetry, thermomechanical analysis and dilatometry, and thermogravimetry. This book is intended for the senior undergraduate or beginning graduate student, as well as for the researcher and teacher interested in thermal analysis.




Thermal Analysis


Book Description

Thermal Analysis




Thermal Analysis of Polymeric Materials


Book Description

Table of Contents Table of Contents 1 Atoms, small, and large molecules 2 Basics of thermal analysis 3 Dynamics of chemical and phase changes 4 Thermal analysis tools 5 Structure and properties of materials 6 Single component materials 7 Multiple component materials App. A.1 Table of thermal properties of linear macromolecules and related small molecules - the ATHAS data bank App. A.2 Radiation scattering App. A.3 Derivation of the Rayleigh ratio App. A.4 Neural network predictions App. A.5 Legendre transformations, Maxwell relations, linking of entropy and probability, and derivation of (dS/dT) App. A.6 Boltzmann distribution, harmonic vibration, complex numbers, and normal modes App. A.7 Summary of the basic kinetics of chemical reactions App. A.8 The ITS 1990 and the Krypton-86 length standard App. A.9 Development of classical DTA to DSC App. A.10 Examples of DTA and DSC under extreme conditions App. A.11 Description of an online correction of the heat-flow rate App. A.12 Derivation of the heat-flow equations App. A.13 Description of sawtooth-modulation response App. A.14 An introduction to group theory, definitions of configurations and conformations, and a summary of rational and irrational numbers App. A.15 Summary of birefringence and polarizing microscopy App. A.16 Summary of X-ray diffraction and interference effects App. A.17 Optical analog of electron double diffraction to produce Moire patterns.




Handbook of Thermal Analysis and Calorimetry


Book Description

Handbook of Thermal Analysis and Calorimetry, Volume 1: Principles and Practice describes the basic background information common to thermal analysis and calorimetry in general. Thermodynamic and kinetic principles are discussed along with the instrumentation and methodology associated with thermoanalytical and calorimetric techniques. The purpose is to collect the discussion of these general principles and minimize redundancies in the subsequent volumes that are concerned with the applications of these principles and methods. More unique methods, which pertain to specific processes or materials, are covered in later volumes.




Handbook of Thermal Analysis and Calorimetry


Book Description

Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. - Features 19 all-new chapters to bring readers up to date on the current status of the field - Provides a broad overview of recent progress in the most popular techniques and applications - Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry - Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics - Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications




Thermal Analysis


Book Description

This textbook provides newcomers to Thermal Analysis with a comprehensive introduction to the basic principles of the technique, such as instrument operation, sample preparation, optimization of operating conditions and a guide to interpreting results. The principal techniques are covered and their performance evaluated, and throughout the emphasis is on the practicalities, with the mathematics kept to a minimum.







Differential Thermal Analysis


Book Description




Thermal Analysis and Design of Passive Solar Buildings


Book Description

Passive solar design techniques are becoming increasingly important in building design. This design reference book takes the building engineer or physicist step-by-step through the thermal analysis and design of passive solar buildings. In particular it emphasises two important topics: the maximum utilization of available solar energy and thermal storage, and the sizing of an appropriate auxiliary heating/cooling system in conjunction with good thermal control. Thermal Analysis and Design of Passive Solar Buildings is an important contribution towards the optimization of buildings as systems that act as natural filters between the indoor and outdoor environments, while maximizing the utilization of solar energy. As such it will be an essential source of information to engineers, architects, HVAC engineers and building physicists.